中国纤检2024,Issue(9) :68-72.

高效液相色谱法测定纺织品中的甲酚曲唑

Determination of drometrizole in textiles by liquid chromatography

冯徐根 韩军 蔚彪
中国纤检2024,Issue(9) :68-72.

高效液相色谱法测定纺织品中的甲酚曲唑

Determination of drometrizole in textiles by liquid chromatography

冯徐根 1韩军 1蔚彪1
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作者信息

  • 1. 北京市产品质量监督检验研究院、国家纺织及皮革产品质量检验检测中心,北京 100025
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摘要

建立了高效液相色谱法测定纺织品中甲酚曲唑的分析方法,以乙腈为萃取溶剂,采用超声萃取法提取纺织品中的甲酚曲唑,优化了仪器分析条件和样品前处理条件.结果表明:方法线性范围10 μg/mL~50 μg/mL,检出限为21.2mg/kg,加标回收率为94.1%~97.4%,相对标准偏差为3.4%~5.9%.本方法操作简便、分析快速,适用于纺织品中甲酚曲唑的检测.

Abstract

Established the analysis methods of drometrizole in textiles,Acetonitrile was used as the extraction solvent,and ultrasonic extraction was used to extract drometrizole from textiles.Optimized instrument analysis conditions.The results indicate that the linear range of the method is 10~50 μg/mL,the detection limits of the method are 21.2 mg/kg,the recoveries range from 94.1%to 97.4%,and the relative standard deviation is at the range of 3.4%to 5.9%.This method is easy to operate and fast to analyze and is suitable for the detection of drometrizole in textiles.

关键词

纺织品/防晒服/甲酚曲唑/紫外线吸收剂/液相色谱

Key words

textiles/UV-protection clothes/drometrizole/ultraviolet absorbents/HPLC

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出版年

2024
中国纤检
中国纤维检验局

中国纤检

影响因子:0.11
ISSN:1671-4466
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