真空2024,Vol.61Issue(1) :68-73.DOI:10.13385/j.cnki.vacuum.2024.01.11

一种基于无转移PMMA和PI的渗透性标准漏孔的氦气渗透性能研究

Helium Permeation Performance Study of a Permeable Standard Leak Element Based on Transfer-free PMMA and PI

方庆国 王宗林 张俊 王旭迪
真空2024,Vol.61Issue(1) :68-73.DOI:10.13385/j.cnki.vacuum.2024.01.11

一种基于无转移PMMA和PI的渗透性标准漏孔的氦气渗透性能研究

Helium Permeation Performance Study of a Permeable Standard Leak Element Based on Transfer-free PMMA and PI

方庆国 1王宗林 1张俊 1王旭迪1
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作者信息

  • 1. 合肥工业大学机械工程学院,安徽 合肥 230009
  • 折叠

摘要

研制了一种基于无转移聚甲基丙烯酸甲酯(PMMA)或聚酰亚胺(PI)的漏孔元件.通过在铜箔上旋涂PMMA或PI,另一面旋涂光刻胶,并利用紫外光刻打孔,在铜箔上刻蚀出了不同阵列的直径约10 μm的小孔.基于差压法测量了氦气通过该标准漏孔元件的流导.结果表明:在从5 kPa到105Pa压力范围内,各测试样品均表现出分子流动状态;无转移PMMA或PI的流导和有效渗透面积呈线性关系,可通过控制小孔数量来控制PMMA或PI的有效渗透面积,从而获得不同的流导;所开发的无转移PMMA或PI为优良的低渗透漏孔理想材料.

Abstract

A standard leak element based on transfer-free polymethylmethacrylate(PMMA)or polyimide(PI)was developed.The fabrication process involved spin-coating PMMA or PI on a copper foil,followed by spin-coating photoresist on the opposite side,and subsequently creating small holes of different arrays with a diameter of about 10 μm on the copper foil using UV lithography.The flow conductance of helium through the leak element was measured by the differential pressure method.The results show that the samples all exhibite a molecular flow regime within the pressure range from 5 kPa to 105 Pa.The flow conductance of transfer-free PMMA or PI shows a linear relationship with the effective permeation area,and the effective permeability area of PMMA or PI can be controlled by controlling the number of small holes,thereby obtaining different flow conductance.The transfer-free PMMA or PI materials developed in this study are ideal for low-permeation leak elements.

关键词

无转移/聚甲基丙烯酸甲酯/聚酰亚胺/渗透型漏孔/恒定流导

Key words

transfer-free/PMMA/PI/permeation leak/constant conductance

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基金项目

国家自然科学基金项目(62201188)

出版年

2024
真空
中国机械工业集团公司沈阳真空技术研究所

真空

CSTPCD
影响因子:0.926
ISSN:1002-0322
参考文献量7
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