首页|莫来石纤维含量对激光选区烧结结合真空浸渗制备二氧化硅陶瓷型芯性能的影响

莫来石纤维含量对激光选区烧结结合真空浸渗制备二氧化硅陶瓷型芯性能的影响

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二氧化硅(SiO2)陶瓷型芯热膨胀系数低、烧结温度低,具有优异的酸碱浸出能力,是生产涡轮空心叶片的必要材料。传统工艺在成形陶瓷型芯时受到模具限制,部分复杂结构陶瓷型芯甚至难以制造,生产高质量复杂结构陶瓷型芯面临挑战。采用激光选区烧结技术(SLS)和真空浸渗工艺(VI)相结合的方法制备SiO2 陶瓷型芯。应用莫来石纤维作为增强相,分析了莫来石纤维对SiO2 晶粒烧结过程的干扰及其在层间的堆积所引发的分层现象,阐明了莫来石纤维含量对SLS-VI制备SiO2 陶瓷型芯性能的影响规律,探究出当纤维含量为 1%(质量分数)时陶瓷型芯综合性能最好,孔隙率为 31。16%,室温抗弯强度为 15。23 MPa,高温抗弯强度为 22。91 MPa。
Effect of Mullite Fiber Content on the Properties of Silica Ceramic Cores Prepared by Selective Laser Sintering Combined with Vacuum Infiltration
Silicon dioxide(SiO2)ceramic cores are essential for manufacturing turbine hollow blades because of their low thermal expansion coefficient,low sintering temperature,and excellent acid-base leaching resistance.The traditional process is limited by the use of molds when forming ceramic cores.Some complex structural ceramic cores are even difficult to manufacture,and the production of high-quality complex structural ceramic cores is challenging.In this study,SiO2 ceramic cores were prepared via a combination of selective laser sintering(SLS)and vacuum infiltration(VI)techniques.Mullite fibers were used as the reinforcing phase,the interference of mullite fibers on the sintering process of SiO2 grains and the delamination phenomenon caused by the accumulation between layers were then analysed,and the influence of the mullite fiber content on the properties of the SiO2 ceramic core prepared by SLS-VI was clarified.The comprehensive performance of the ceramic core is the best when the fiber content is 1 wt.%,with a porosity of 31.16%,a flexural strength at room temperature of 15.23 MPa,and a flexural strength at high temperature of 22.91 MPa.

SiO2 ceramic coresselective laser sinteringvacuum infiltrationmullite fiber contentsmechanical properties

刘珩、刘翰帝、张任重、吴甲民、闫春泽、文世峰、陈超越、任忠鸣、史玉升

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华中科技大学材料科学与工程学院材料加工与模具技术全国重点实验室,湖北 武汉 430074

增材制造陶瓷材料教育部工程研究中心,湖北 武汉 430074

温州HUST先进制造研究所微波通信材料与设备重点实验室,浙江 温州 325035

上海大学材料科学与工程学院省部共建高品质特殊钢冶金与制备国家重点实验室,上海 200444

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SiO2陶瓷型芯 激光选区烧结技术 真空浸渗工艺 莫来石纤维 力学性能

2025

铸造技术
西安市科学技术协会

铸造技术

影响因子:0.458
ISSN:1000-8365
年,卷(期):2025.46(1)