造纸科学与技术2024,Vol.43Issue(2) :33-38.DOI:10.19696/j.issn1671-4571.2024.2.007

荛花韧皮部制浆工艺优化及纸浆性能研究

Research on Optimization of the Pulping Process of Wikstroemia Bast and Its Pulp Properties

黄虎 李兵云 李海龙 柴若雪
造纸科学与技术2024,Vol.43Issue(2) :33-38.DOI:10.19696/j.issn1671-4571.2024.2.007

荛花韧皮部制浆工艺优化及纸浆性能研究

Research on Optimization of the Pulping Process of Wikstroemia Bast and Its Pulp Properties

黄虎 1李兵云 1李海龙 1柴若雪1
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作者信息

  • 1. 华南理工大学 造纸与污染控制国家工程研究中心,广东 广州,510640
  • 折叠

摘要

以荛花韧皮部为研究对象,分析了韧皮部的化学组分含量,初步对比了五种不同制浆方法对纸浆性能的影响,从而选择出荛花韧皮部合适的制浆方法,并优化其制浆工艺.实验结果表明,荛花韧皮部硝酸乙醇纤维素含量为54.6%,木素含量为 8.7%,果胶含量为18.1%,苯醇抽出物为 2.6%;与其他四种制浆方法相比,AS-AQ制浆方法在制浆得率及纸浆卡伯值、特性黏度、白度等方面较有优势,因此荛花韧皮部采用AS-AQ法制浆较为合适,其最佳的制浆工艺条件为:用碱量14%,亚硫酸化度80%,升温时间1.5 h,保温时间3 h,最高温度 140℃,液比 1∶5;在此工艺条件下浆料得率为 60.1%,卡伯值为 9.66,特性黏度为 1115 mL/g,白度为 44.74%ISO.

Abstract

In this paper,the chemical component content of Wikstroemia bast was analyzed,and the effects of five different pulping methods on the pulp properties were compared in order to select the appropriate pulping method for the Wikstroemia bast and optimize the pulping process.The experimental results showed that the nitrate ethanol cellulose was 54.6%,the lignin content was 8.7%,the pectin content was 18.1%,and the benzene-alcohol extractive content was 2.6%.Compared with the other five pulping methods,the AS-AQ pulping method had advantages in pulp yield,Kappa number,intrinsic viscosity and brightness.The optimal conditions of the pulping process are:alkali charge 14%,the degree of sulfitation 80%,the maximum temperature 140 °C,time at the heating time 1.5 h,time at the cooking temperature 3 h,and the ratio of solid to liquid 1∶5.Under the optimal conditions,the pulp yield was 60.1%,and the Kappa number was 9.7,and the intrinsic viscosity was 1115 mL/g,and the brightness was 44.7%ISO.

关键词

荛花/韧皮纤维/制浆/纸张性能

Key words

wikstroemia/bast fiber/pulping/paper performance

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基金项目

国家科技基础资源调查专项(2019FY100900)

出版年

2024
造纸科学与技术
广东省造纸学会 广东省造纸研究所

造纸科学与技术

CSTPCD
影响因子:0.269
ISSN:1671-4571
参考文献量20
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