首页|高效固结矿用抑尘剂的制备与性能研究

高效固结矿用抑尘剂的制备与性能研究

扫码查看
为抑制煤炭开采和运输过程中煤尘逸散,减少其对井下生产环境以及工人的身体健康造成危害,选取十二烷基磺酸钠(SDS)、椰油酰两性基二乙酸二钠(CAD)以及脂肪醇聚氧乙烯醚7(AEO-7)3种表面活性剂,通过表面张力试验筛选出性能优异的CAD和AEO-7.同时,选取环保可降解黏结剂甲基纤维素(MC)、羧甲基淀粉钠(CMS-Na)和聚乙烯醇(PVA),以黏度试验为依据筛选出具有良好黏结性能的MC.在此基础上,利用以硬度和渗透深度为评价指标的正交试验法分析获得抑尘剂的最佳配方为0.06%CAD+0.10%AEO-7+0.20%MC.基于所得最佳配方抑尘剂的润湿、保水以及固结方面的性能进行评价,接触角测试得到抑尘剂与煤尘的接触角为36.5°,具有良好的润湿能力;8 h内的累计蒸发量为4 g且形成的固化层硬度可达到76.4 HA,在经过10 m/s风流扰动后,煤样的风蚀率为2.23%.结合扫描电镜分析在放大1 000倍时喷洒抑尘剂后煤尘颗粒表面的微观形态,发现煤尘粒径可达60 μm左右,进行了有效的团聚行为,同时粒径实验也证明抑尘剂对煤尘进行了有效的润湿团聚行为,增加了煤尘重力与密度,显著提高抑尘效果.
Preparation and performance study of efficient consolidating dust suppressants for mine production
In order to reduce the coal dust caused by the mining and transportation process in the coal mine into the air and avoid its harm to the underground production environment and the health of workers,three surfactants,including sodium dodecyl sulfonate(SDS),disodium cocoamphodiacetate(CAD)and fatty alcohol polyoxyethylene ether 7(AEO-7),were selected,and CAD and AEO-7 with excellent performance were screened out by surface tension experiment.At the same time,environmentally friendly degradable bind-ers methylcellulose(MC),sodium carboxymethyl starch(CMS-Na)and polyvinyl alcohol(PVA)were selected to screen out(MC)with good adhesion performance based on viscosity experiment.On this basis,the orthogonal test method with hardness and penetration depth as the evaluation index was used to analyze and obtain the optimal formula of dust suppressant as 0.06%CAD+0.10%AEO-7+0.20%MC.Based on the evaluation of the wetting,water retention,and solidification performance of the obtained optimal formula dust suppres-sant,the contact angle test showed that the contact angle between the dust suppressant and coal dust was 36.5°,indicating good wetting ability.The cumulative evaporation within 8 hours is 4 g and the hardness of the solidified layer formed can reach 76.4 HA.After being disturbed by a 10 m/s airflow,the wind erosion rate of the coal sample is 2.23%.Combined with scanning electron microscopy to ana-lyze the micromorphology of coal dust particles after spraying dust suppressant at 1 000 times magnification,it was found that the parti-cle size of coal dust can reach about 60 μm,and effective agglomeration behavior was carried out,and the particle size test also proved that the dust suppressant had an effective wetting and agglomeration behavior on coal dust,increasing the gravity and density of coal dust and significantly improving the dust suppression effect.

coal dustbond curingorthogonal experimentperformance testing

汪志强、刘涛

展开 >

国能乌海能源黄白茨矿业有限责任公司,内蒙古乌海 016040

中煤科工集团重庆研究院有限公司,重庆 400037

煤尘 黏结固化 正交实验 性能测试

国家重点研发计划重庆市自然科学基金面上项目

2017YFC0805202cstc2021jcyjmsxmX1184

2024

能源与环保
河南省煤炭科学研究院有限公司 河南省煤炭学会

能源与环保

CSTPCD
影响因子:0.221
ISSN:1003-0506
年,卷(期):2024.46(5)