首页|Modification of cold-sprayed high-entropy alloy particles reinforced aluminum matrix composites via friction stir processing
Modification of cold-sprayed high-entropy alloy particles reinforced aluminum matrix composites via friction stir processing
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NSTL
Elsevier
? 2022 Elsevier B.V.In this study, a kind of novel Al matrix composite reinforced by CoCrFeNi HEA particles was fabricated by cold spray (CS) and subsequent friction stir processing (FSP) for the first time. The microstructure and mechanical properties of cold-sprayed (CSed) and friction stir processed (FSPed) CoCrFeNip/6061Al composites were examined using scanning electron microscopy, energy dispersive spectroscopy, electron backscattering diffraction, X-ray diffraction, and hardness and tensile tests. The results demonstrated that CSed samples exhibited a number of micro-pores in the Al matrix with homogeneous distribution of HEA particles, but heterogeneously distributed grain size. Continuous dynamic recrystallization and geometric dynamic recrystallization occurred at the interface between the HEA particles and Al matrix. Following FSP, the micro-pores were eliminated, and a small amount of HEA particles was fragmented and uniformly dispersed in the Al matrix. Moreover, the average size of HEA particles was refined from ~21–14 μm. The Al matrix exhibited dynamic recrystallization and particle-stimulated nucleation recrystallization, thus resulting in an average grain size of ~1.9 μm. Obvious diffusion layers of 0.5 μm and 1 μm in thickness occurred at the interface between the HEA particles and Al matrix in CSed and FSPed samples, respectively. A new phase with a body-centered cubic structure was confirmed to be an HEA in diffusion layers. Compared with CSed samples, the microhardness, ultimate tensile strength, and elongation of the FSPed samples increased by 91%, 60%, and 130%, respectively. The improved mechanical properties are attributed to the high density and enhanced interfacial bonding. Thus, this study provided a novel method for preparing high-performance Al matrix composites reinforced by HEA particles.
Al matrix compositeCold sprayFriction stir processingHigh-entropy alloyMicrostructure
Han P.、Wang W.、Liu Z.、Zhang T.、Liu Q.、Guan X.、Qiao K.、Ye D.、Cai J.、Wang K.、Xie Y.
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School of Metallurgical Engineering National and Local Joint Engineering Research Center for Functional Materials Processing Xi'an University of Architecture and Technology
The Key Lab of Guangdong for Modern Surface Engineering Technology National Engineering Laboratory for Modern Materials Surface Engineering Technology Institute of New Materials Guangdong Academy of Sciences
NSTL
Elsevier
