首页|Fabrication of a micro gas chromatography column via the layer-by-layer deposition of mesoporous silica as the stationary phase
Fabrication of a micro gas chromatography column via the layer-by-layer deposition of mesoporous silica as the stationary phase
扫码查看
点击上方二维码区域，可以放大扫码查看
原文链接
NSTL
Elsevier
? 2022In this paper, a micro gas chromatographic column (μGCC) was fabricated via the layer-by-layer (LBL) deposition of mesoporous silica (MS) as the stationary phase. The μGCC with embedded elliptical-cylindrical posts was fabricated by typical micro-electro-mechanical system (MEMS) techniques. The MS powder was prepared by a sol-gel method and then deposited inside the microchannels of the μGCC by LBL deposition. This process avoided the high temperature required for the sol-gel method to directly prepare MS inside the microchannel surfaces of the μGCC. Mixtures of light alkanes (C1–C4) could be separated in the μGCC. The separation results showed that the resolution between the components of the sample increased with the number of deposition cycles. When the number of deposition cycles increased from 1 to 8, the resolution of methane and ethane was increased from unseparated to 5.89.
Layer-by-layer depositionMesoporous silicaMicro-electro-mechanical system
Zhang H.、Feng F.、Zhao Y.、Zhao B.、Li L.、Li X.、Zheng D.
展开 >
State Key Laboratory of Transducer Technology Shanghai Institute of Microsystem and Information Technology Chinese Academy of Sciences
NSTL
Elsevier
