首页|Comparison of three stationary phases in the separation of polyphenyls by liquid chromatography
Comparison of three stationary phases in the separation of polyphenyls by liquid chromatography
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NSTL
Elsevier
We present herein new analytical protocols for the separation and structural elucidation of polyphenyls. Three commercially available chromatographic stationary phases are compared in the separation of these non-polar, unfunctionalized, positional isomers. Baseline separation of nine terphenyl and quaterphenyl isomers is achieved in under ten minutes using a rapid gradient elution HPLC method. Complete separation of these, and a further five polyphenyls, is demonstrated. We finally present a linear correlation between solvent accessible surface area and the retention times of these closely related compounds. (c) 2022 Elsevier B.V. All rights reserved.
NSTL
Elsevier
