首页|Al-Permalloy (Ni71.25Fe23.75M5) obtained by mechanical alloying. The ~ influence of the processing parameters on structural, microstructural, thermal, and magnetic characteristics

Al-Permalloy (Ni71.25Fe23.75M5) obtained by mechanical alloying. The ~ influence of the processing parameters on structural, microstructural, thermal, and magnetic characteristics

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A new alloy, permalloy alloyed with aluminum, has been obtained by mechanical alloying using elemental powders as raw materials. The new alloy was obtained in powder form by adding an amount of 5 wt% of Al to permalloy (75% Ni and 25% Fe, wt.%) resulting Al-Permalloy with Ni71.25Fe23.75A15 composition. The alloy was obtained using different ball to powder ratio (BPR): 4:1, 8:1 and 17:1 and keeping the rest of the mechanical alloying/milling parameter constant. The BPR influences the time required for the alloy synthesis and alloy characteristics. The time required for alloy synthesis as FCC single phase varies from 4 h when using a BPR of 17:1 to 8 h when using a BPR of 4:1. A more compact cubic structure is obtained when using a BPR of 8:1. The particles are flattened for all BPRs used, but upon changing the BPRs particles shape is changing and become more or less flattened. Large particles have been obtained when using BPRs of 4:1 and 17:1 and finer particles when using a BPR of 8:1. Curie temperature of the Al-Permalloy is depending on synthesis conditions varying from 478 °C to 501 °C. The higher saturation magnetization has been found when using a BPR of 8:1. The powder characteristics evolution upon increasing the milling time for all three BPRs is discussed in the light of X-ray diffraction, scanning electron microscopy, energy dispersive X-ray spectrometry, differential scanning calorimetry, particles size analyses and magnetic investigation.

PermalloyMechanical millingMagnetic materialAl-PermalloyBall to powder ratio BPR

Traian Florin Marinca、Andrei loan Sule、Razvan Hirian

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Materials Science and Engineering Department, Technical University of Cluj-Napoca, 103-105 Muncii Aveenue, 400641 Cluj-Napoca, Romania

Babes-Bolyai University, Faculty of Physics, 400084 Cluj-Napoca, Romania

2022

Advanced Powder Technology

Advanced Powder Technology

EISCI
ISSN:0921-8831
年,卷(期):2022.33(7)
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