首页|微波辅助法提取宁夏黄芪中主要微量元素的工艺研究

微波辅助法提取宁夏黄芪中主要微量元素的工艺研究

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[目的]优化宁夏黄芪中主要微量元素的提取工艺.[方法]采用微波提取法宁夏黄芪中铜、铁、锌、钙,火焰原子吸收光谱法测定其含量,并利用正交试验优化宁夏黄芪中4种元素的提取工艺.[结果]选择水作为提取溶剂,以Cu、Zn含量测定结果为依据,正交试验优化所得的提取最佳条件为:料液比1∶5.0,提取时间10 min,微波功率480W;在此条件下,重复试验取得了良好效果.[结论]研究结果为全面了解宁夏黄芪的质量提供了理论依据.
Study on the Technology of Extracting Microelements of Astragalus from Ningxia by Microwave-assisted Method
[Objective] To optimize the extracting process of microelements of Astragalus from Ningxia. [ Method] The essential micro elements such as Cu, Fe, Zn and Ca from Astragalus in Ningxia was extracted by Microwave assisted extraction ( MAE) , and their contents were determined by Flame Atomic Absorption Spectrometry(FAAS)method. [Result] Taking water as solvent, the contents of Cu, Zn as measure basis, the best process which were optimized by orthogonal experiments was 1:5.0 of solid-liquid radio, 10 min of extraction time, 480 W of microwave power; under these conditions, extraction effect of the microelement in Astragalus from Ningxia was good. [ Conclusion] These pri mary research results provided the theoretic basis to understand the quality of Astragalus from Ningxia comprehensively.

AstragalusMicroelementsMAEFAASOrthogonal experiment

丁润梅、田大年

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宁夏医科大学高等卫生职业技术学院,宁夏银川750004

宁夏医科大学公共卫生学院,宁夏银川750004

黄芪 微量元素 微波辅助提取法 火焰原子吸收光谱法 正交试验

2010宁夏高等学校科研项目宁夏医科大学青年基金

宁教高[2010]297号XQ200916

2011

安徽农业科学
安徽省农业科学院

安徽农业科学

影响因子:0.413
ISSN:0517-6611
年,卷(期):2011.39(21)
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