油茶子的超临界萃取及其萃取物的组分分析
Supercritical Extraction of Oil-tea Camellia Seeds and Component Analysis of Its Extracts
崔朋 1方红霞 1吴有娣 2韩信 2刘良欢2
作者信息
- 1. 黄山学院应用化学研究所,安徽黄山245041
- 2. 黄山学院化学化工学院,安徽黄山245041
- 折叠
摘要
[目的]探索分析油茶子萃取物的组分.[方法]以油茶子为原料,采用超临界CO2萃取法对油茶子进行萃取,并采用高效液相色谱(HPLC)和气相色谱-质谱联用(GC-MS)分析萃取物的组分.[结果]油茶子的超临界CO2萃取产率几乎不受温度的影响,与萃取压力呈正相关,在同等务件下压力越大,产率越高.从HPLC和GC-MS图谱分析,不同方法萃取的油茶子的化学组分没有明显的区别.[结论]通过对油茶子的超临界萃取物进行测试,为油茶子中有效成分的提取分离提供参考.
Abstract
[Objective] To explore the main components of oil-tea camellia seeds.[Method] With oil-tea camellia seeds as the raw materials,CO2 supercritical extraction was carried out.The components of extracts were analyzed by HPLC and GC-MS.[Result] The extraction yield was not affected by temperature,but had positive correlation with extraction pressure.Under the same conditions,the extraction yield enhanced with the increase of extraction pressure.Analysis of HPLC and GC-MS spectra showed that there were no obvious differences in the chemical components of oil-tea camellia seeds by different methods.[Conclusion] Supercritical extraction of oil-tea camellia seeds provides references for the extraction and isolation of effective components in oil-tea camellia seeds.
关键词
油茶子/超临界/高效液相色谱/气质联用Key words
Oil-tea camellia seeds/Supercritical/HPLC/GC-MS引用本文复制引用
基金项目
国家级大学生创新创业训练计划项目(15362)
出版年
2016
国家科技期刊平台
NSTL
维普
万方数据