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中药枇杷花药用部位表述的合理性研究

Research on the Rationality of Describing the Medicinal Parts of Loquat Flower

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[目的]研究中药枇杷花药用部位与非药用部位的差异,以及非药用部位混入的影响.[方法]色谱柱SHIMSEN Anklyo C18(4.6 mm×100 mm,5 μm),流动相为甲醇(A)-0.1%醋酸铵溶液(B),梯度洗脱;流速1.0 mL/min;检测波长210、355 nm;柱温35℃;进样量10 μL;测定中药枇杷花药用部位和非药用部位中金丝桃苷、异槲皮苷、槲皮苷、槲皮素、熊果酸、齐墩果酸、科罗索酸这7 种成分的含量,并对数据进行分析.[结果]枇杷花的花和花蕾中各成分的含量和分布规律较为接近;其他部位中各成分的含量和分布规律与枇杷花的花或花蕾比较具有一定差异.[结论]枇杷花的药用部位表述为"干燥带花蕾的花序"要更为清晰合理.
[Objective]To study the differences between medicinal and non medicinal parts of loquat flowers,as well as the effects of mixing non medicinal parts.[Method]HPLC was performed on a column of SHIMSEN Anklyo C18(4.6 mm×100 mm,5 μm)using methanol(A)and 0.1%ammonium acetate(B)as the mobile phase in a gradient elution;the flow rate was 1.0 mL/min;the detection wavelength was 210 and 355 nm;the column temperature was 35 ℃ and the injection volume was 10 μL;determined the content of seven chemical components,inclu-ding hyperoside,isoquercitrin,quercitrin,quercetin,ursolic acid,oleanolic acid and corosolic acid,in the medicinal and non medicinal parts of loquat flowers;and analyzed the data.[Result]The content and distribution patterns of various chemical components in the flowers and buds of loquat flowers were relatively similar;there were certain differences in the content and distribution patterns of various chemical components in other parts compared to the flowers or buds of loquat flowers.[Conclusion]The medicinal part of loquat flowers is more clearly and reasonably described as a"dry inflorescence with buds".

Loquat flowersActive ingredientsMedicinal partsNon medicinal parts

胡孔兴、何鹏

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芜湖市食品药品检验中心,安徽芜湖 241000

枇杷花 活性成分 药用部位 非药用部位

2024

安徽农业科学
安徽省农业科学院

安徽农业科学

影响因子:0.413
ISSN:0517-6611
年,卷(期):2024.52(22)