首页|基于QDA与GC-IMS技术分析不同油脂热加工处理对松茸风味的影响

基于QDA与GC-IMS技术分析不同油脂热加工处理对松茸风味的影响

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为辨别不同油脂加工处理对松茸风味特征的影响,分别以黄油、橄榄油、猪油煎制鲜松茸,通过感官定量描述评价(Quantitative descriptive analysis,QDA)与气相色谱-离子迁移谱技术(Gas chro-matography-ion mobility spectrometry,GC-IMS)结合分析挥发性风味化合物变化,并采用主成分、聚类、热图、相对气味活度值、正交偏最小二乘法等多元化学统计法分析油脂对松茸风味的影响.结果表明:黄油加工的松茸呈现较好的爆米花香气和蘑菇气味,橄榄油加工的松茸风味较清淡,猪油加工使松茸汽柴油特征风味更加突出.GC-IMS共鉴定出47种挥发性风味化合物,经油脂煎制后的松茸主要挥发性风味化合物为酮类(相对含量31.30%~36.26%)和醇类(相对含量26.64%~28.92%);ROAV值>1的挥发性风味化合物共有24种,其中3-辛酮(D)对风味影响最大.黄油加工处理使样品中2-甲基吡嗪(ROAV值为21.8,是橄榄油加工组的1.59倍)呈现较好的爆米花香,2-庚醇(ROAV值为11.2,是猪油加工组的1.5倍)呈现较好的蘑菇香,2-辛酮(ROAV值为5.8,是橄榄油加工组的1.9倍)呈现较好的汽柴油特征风味.综上,植物性油脂加工对松茸风味影响较小,动物性油脂影响较大.研究结果可以为松茸风味品质调控提供参考.
Effects of Different Oil Thermal Processing Treatments on the Flavors of Matsutake Analyzed Based on QDA and GC-IMS Techniques
This study aimed to identify the effects of different oil processing treatments on the flavor characteristics of matsutake.Fresh matsutake mushrooms were fried with butter,olive oil and lard respectively,quantitative de-scriptive analysis(QDA)and gas chromatography-ion mobility spectrometry(GC-IMS)were applied to analyze the changes of volatile flavor compounds.The effects of oil treatments on the flavors of matsutake mushrooms were an-alyzed by multivariate chemical statistical methods such as principal component,clustering,heat map,relative odor activity value and orthogonal partial least square methods.The results showed that butter processed matsutake pre-sented better popcorn and mushroom odors,olive oil processed matsutake showed lighter flavors,and lard processed matsutake could make the characteristic flavors of diesel and gasoline more prominent.Besides,a total of 47 volatile flavor compounds were identified by GC-IMS,and the main compounds of matsutake after oil frying were ketones(31.30%~36.26%)and alcohols(26.64%~28.92%).There were 24 volatile flavor compounds with ROAV>1,among which 3-octanone(D)presented the greatest effects on the flavors.Butter processing resulted in better popcorn flavor with 2-methylpyrazine(ROAV=21.8,1.59 times that of olive oil processing),better mushroom flavor with 2-heptol(ROAV=11.2,1.5 times that of lard processing),and better gasoline and diesel characteristic flavors with 2-octanone(ROAV=5.8,1.9 times that of olive oil processing).In conclusion,the processing of vegetable oil had little effects on the flavors of matsutake,while the processing of animal oil presented greater effects.These results can provide refer-ences for regulating the flavor qualities of matsutake mushrooms.

matsutakeoilquantitative sensory descriptiongas chromatography-ion mobility spectrometrycom-poundsmultivariate chemical statistics

杨正瑞、易宇文、朱开宪、邓静、乔明锋、蔡雪梅、顾思远、张浩

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四川旅游学院烹饪科学四川省高等学校重点实验室,四川 成都 610100

川菜人工智能重点实验室,四川 成都 610100

四川旅游学院烹饪与食品科学工程学院,四川 成都 610100

松茸 油脂 感官定量描述 气相色谱-离子迁移谱 化合物 多元化学统计法

2025

保鲜与加工
国家农产品保鲜工程技术研究中心(天津)

保鲜与加工

北大核心
影响因子:0.956
ISSN:1009-6221
年,卷(期):2025.25(1)