首页|In3+取代对NiZn微波多晶铁氧体材料电磁性能的影响

In3+取代对NiZn微波多晶铁氧体材料电磁性能的影响

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采用普通陶瓷工艺制备微波多晶尖晶石NiZnIn铁氧体材料,研究了In3+取代对材料微观结构、电磁性能的影响.结果表明,当In3+取代量x在0~0.2范围时,材料的饱和磁化强度4πMs变化很小,气孔率p略有降低,铁磁共振线宽ΔH以各向异性致宽ΔHa为主;当x>0.2后,材料的饱和磁化强度4πMs明显降低,气孔率p增大,铁磁共振线宽ΔH以气孔致宽ΔHp为主.In3+取代NiZn铁氧体使材料的铁磁共振线宽ΔH明显降低,介电损耗角正切tanδε降低至0.5×10-4以下,居里温度近似线性下降.In3+取代NiZn铁氧体烧结温度范围宽,在1200~1240℃温度下烧结,材料的4πMs、ΔH、tanδε变化均较小,工艺实现容易.
Effect of substitutions of In3+ions on the electromagnetic properties of NiZn microwave polycrystalline ferrite materials
Microwave polycrystalline spinel NiZn ferrite materials were prepared by common ceramic process.The effects of substitutions of In3+ions on the microstructure and electromagnetic properties of NiZn ferrite materials were studied.The results show that when the substitution amount x of In3+ion is in the range of 0-0.2,the saturation magnetization of the material changes very little at 4πMs,the porosity p slightly decreases,and the ferromagnetic resonance linewidth of the material ΔH-broadening with anisotropy ΔHa is the main factor;When x>0.2,the saturation magnetization of the material decreases significantly by 4πMs,the porosity p increases,and the ferromagnetic resonance linewidth of the material increases ΔH widens with pores ΔHp is the main focus.Replacing NiZn ferrite with In3+enhances the ferromagnetic resonance linewidth of the material ΔH significantly decreases,and the dielectric loss angle tangent tanδε reduce to 0.5×10-4,the Curie temperature approximately decreases linearly.The sintering temperature range of In3+substituted NiZn ferrite is wide,and sintering at temperatures ranging from 1200 to 1240℃,results in 4πMs,ΔH and tanδε changes are relatively small,and the process implementation is easy.

microwave polycrystalline spinel ferrite materialsubstitutions of In3+ionssaturation magnetizationferromagnetic resonance linewidthdielectric lossCurie temperature

冯涛、袁红兰、陈戈、杨菲、胡家旭

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中国电子科技集团公司第九研究所,四川 绵阳 621000

微波多晶尖晶石铁氧体材料 In3+取代 饱和磁化强度 铁磁共振线宽 介电损耗 居里温度

2024

磁性材料及器件
中国西南应用磁学研究所

磁性材料及器件

影响因子:0.358
ISSN:1001-3830
年,卷(期):2024.55(6)