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鸡骨草中常用农药的检测及残留风险评估

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建立了鸡骨草中常用农药残留的分析方法,并进行了残留量风险评估.采用QuEChERS法净化、UPLC-MS/MS法对 50 批鸡骨草中 11 种农药进行测定;点评估模式计算长期摄入风险,以ADI表示;危险指数法评估多农药残留的联合暴露风险,以 HI 表示;借鉴兽药残留风险排序矩阵计算农药残留风险得分.结果表明:11 种农药组分线性相关系数均>0.990,回收率为 79.1%~117.1%;共检出 5 种农药,其中吡唑醚菌酯检出率最高;ADI为 0.002%~0.048%,HI为 0.001.该分析方法操作简单快速、准确可靠,适用于鸡骨草中农药残留分析测试.
Detection and Risk Assessment of Common Pesticides in Abrus Cantoniensis Hance
An analytical method for commonly used pesticide residues in Abrus cantoniensis Hance was established,and residual risk assessment was carried out.QuEChERS method was used for purification,and 11 pesticides were determined in 50 batches of Abrus cantoniensis Hance by UPLC-MS/MS;the point assessment model was used to calculate the long-term intake risk(ADI);the joint exposure risk of multiple pesticide residues was evaluated using the hazard index method,expressed as HI;using the risk ranking matrix of veterinary drug residues for reference,the risk score of pesticide residues was calculated.The results showed that the linear correlation coefficients of the 11 pesticide components were all greater than 0.990,with recoveries ranging from 79.1%to 117.1%.A total of 5 pesticides were detected,with the highest detection rate of pyraclostrobin;the ADI ranged from 0.002%to 0.048%,and the HI was 0.001.The analysis method is simple,fast,accurate,and reliable,and is suitable for the analysis and testing of pesticide residues in Abrus cantoniensis Hance.

Abrus cantoniensis HanceUUPLC-MS/MSPesticide residuesRisk assessmentRisk for combined exposure

陈凤、梁馨予、陈婷婷、吕好平

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玉林市食品药品检验检测中心,广西 玉林 537000

玉林中药材(含香辛料)质量监测与评价工程技术研究中心,广西 玉林 537000

鸡骨草 UPLC-MS/MS 农药残留 风险评价 联合暴露风险

广西中医药管理局课题项目广西壮族自治区科技厅项目

GXZYZ20210116桂科AD22080002

2024

当代化工
中国石油抚顺石化公司,中国石化抚顺石油化工研究院,沈阳市医药和化工行业联合会

当代化工

CSTPCD
影响因子:0.412
ISSN:1671-0460
年,卷(期):2024.53(6)
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