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耐温水基聚合物压裂液制备及性能评价

Preparation and Performance Evaluation of Temperature-resistant Water-based Polymer Fracturing Fluid

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针对低渗油藏水基压裂液体系进行了实验研究,通过室内性能评价测试优选了耐温水基聚合物压裂液体系配方,结合红外光谱及热重分析等微观手段对其结构、热稳定进行了分析,利用室内评价实验测定了其流变性、携砂性、返排防膨性及滤失性等相关特性,并在油田现场进行了先导性试验.压裂液主体配方(质量分数)为:0.2%~0.8%HPAM稠化剂、1.0%B3黏土稳定剂、0.1%~0.3%M2破胶剂、0.3%G6助排剂、0.2%TB破乳剂及0.02%~0.06%FS交联剂.微观测试结果表明其具备优良的热稳定性.压裂液破胶残渣远低于其他体系,对于黏土质量分数大于18%的岩屑防膨率可以达到88%.压裂液体系不需要额外降滤失剂的添加,对储层的伤害程度相较于胍胶体系压裂液可降低超过10%.
An experimental study was carried out on the water-based fracturing fluid system for low-permeability reservoirs.The formulation of the temperature-resistant water-based polymer fracturing fluid system was preferred through the indoor performance evaluation test,and its structural thermal stability was analyzed by combining infrared spectroscopy and thermogravimetric analysis with other microscopic means,and its rheological,sand-carrying,return-expanding and anti-expansion and filtration-loss properties were determined by using the indoor evaluation experiments,and the pilot tests were carried out on site in the oilfield.The main formulation(mass fraction) of the fracturing fluid was determined as follows:0.2%~0.8% HPAM thickener,1.0% B3 clay stabilizer,0.1%~0.3% M2 glue breaker,0.3% G6 drainage aid,0.2% TB emulsion breaker and 0.02%~0.06% FS crosslinker.The microscopic test results showed that it had excellent thermal stability.Fracturing fluid breakage residue was much lower than other systems,and the anti-expansion rate could reach 88% for rock chips with clay mass fraction more than 18%.The fracturing fluid system did not require the addition of additional filter loss reducers,and the damage to the reservoir could be reduced by more than 10% compared with the guanidine gel system.

Low-permeability reservoirWater-based fracturing fluidTemperature resistancePerformance evaluation

罗梓轩、袁斌、张世阔、邢艳斌、张相春

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西安长庆同欣石油科技有限公司,陕西西安 710016

中石油长庆油田分公司第十二采油厂,甘肃庆阳 745400

中石油长庆油田分公司第十采油厂,甘肃庆阳 745000

西安石油大油气科技有限公司,陕西西安 710061

西安石油大学,陕西西安 710065

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低渗油藏 水基压裂液 耐温 性能评价

国家自然科学基金面上项目

52174027

2024

当代化工
中国石油抚顺石化公司,中国石化抚顺石油化工研究院,沈阳市医药和化工行业联合会

当代化工

CSTPCD
影响因子:0.412
ISSN:1671-0460
年,卷(期):2024.53(9)