当代化工2024,Vol.53Issue(12) :2831-2834.

新型水基钻井液添加剂的合成和性能表征

Synthesis and Characterization of New Water-Based Drilling Fluid Additives

章洋阳 白净 刘锰钰 景瑞
当代化工2024,Vol.53Issue(12) :2831-2834.

新型水基钻井液添加剂的合成和性能表征

Synthesis and Characterization of New Water-Based Drilling Fluid Additives

章洋阳 1白净 1刘锰钰 1景瑞1
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作者信息

  • 1. 西安长庆化工集团有限公司,陕西 西安 710018
  • 折叠

摘要

钻井液的设计和配方对钻井作业的成功有着至关重要的作用,因此对碳酸钙(CaCO3)颗粒作为一种新型水基钻井液添加剂的掺入进行了评估.采用沉淀法合成了一种CaCO3 颗粒,并对其形态、胶体稳定性能和组分结构进行了表征.结果表明:CaCO3 颗粒呈现出典型的方解石菱形形态,粒径分布较窄,平均粒径为2.16 µm;CaCO3 颗粒具有负表面电荷,增加溶液pH会产生过量HCO3-和CO32-以及更多带负表面电荷的离子,代表碳酸盐C—O在1 431 cm-1 附近呈现一条强光谱带;CaCO3 颗粒在25~600℃表现出较高的热稳定性.

Abstract

The design and formulation of drilling fluids play a vital role in the success of drilling operations,and therefore the incorporation of calcium carbonate(CaCO3)particles as a novel water-based drilling fluid additive was evaluated.CaCO3 particles were synthesized using a precipitation method and characterized for its morphology,thermal stability properties and component structure.The results showed that the CaCO3 particles exhibited a typical calcite rhombic morphology with a narrow particle size distribution and an average particle size of 2.16 µm.The CaCO3 particles had negative surface charge,and increasing the solution pH produced excess HCO3-and CO32-ions,as well as more negatively surface-charged ions.The FTIR spectrum presented a strong band around 1 431 cm-1,characteristic of the C—O stretching mode of carbonate.The CaCO3 particles exhibited high-temperature stability in the temperature range from 25℃to 600℃.

关键词

水基钻井液/碳酸钙颗粒/合成/热稳定性/结构

Key words

Water-based drilling fluids/Calcium carbonate particles/Synthesis/Thermal stability/Structure

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出版年

2024
当代化工
中国石油抚顺石化公司,中国石化抚顺石油化工研究院,沈阳市医药和化工行业联合会

当代化工

CSTPCD
影响因子:0.412
ISSN:1671-0460
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