首页|离子色谱法测定地下水中碘离子的方法研究

离子色谱法测定地下水中碘离子的方法研究

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采用离子色谱法测定地下水中碘离子.选择AS19分离柱、电导检测器、阴离子电解再生抑制器电流为99 mA、淋洗液为40 mmol/L KOH溶液、流速为1.00 mL/min、检测器温度为30℃、进样定量环为250 μL.碘离子浓度在0.010 mg/L~1.00 mg/L的范围内与色谱峰面积具有良好的线性关系,其相关系数可以达到0.9998,方法检出限为0.001 mg/L,相对标准偏差为0.4%~8.3%,加标回收率为99.0%~115.0%,有证标准物质分析结果优秀,相对偏差为2.5%.将其应用于地下水中碘离子的测定,结果满意.
The Research of Determination of Iodide in Underground Water by Ion Chromatography
An ion chromatography method for determining iodide in underground water was established.AS19 separation col-umn with conductivity detector was employed.The electric current of anion electrolytic regeneration inhibitor was 99 mA,the eluent was 40 mmol/L KOH solution,the flow rate was 1.00 mUmin,the dectction temperature was 30℃ and the injec-tion volume was 250 μL.The mass concentration of iodide in the range of 0.010 mg/L-1.00 mg/L had good linear relation-ship with the chromatographic peak area,the linear correlation coefficient r was 0.9998.The detection limit was 0.001 mg/L,the relative standard deviations were 0.4%-8.3%,the recovery rates were 99.0%-115.0%,and the analysis results of the certified substances were excellent,its relative deviation was 2.5%.And the determination results of iodide in underground water by the ion chromatography were satisfactory.

Ion ChromatographyIodideUnderground WaterDetermination

黄漂漂

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福建省漳州环境监测中心站,福建 漳州 363000

离子色谱法 碘离子 地下水 测定

2024

福建分析测试
福建省测试技术研究所

福建分析测试

影响因子:0.365
ISSN:1009-8143
年,卷(期):2024.33(2)
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