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超高效液相色谱-串联质谱法测定茶叶中的咖啡因

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采用超高效液相色谱串联质谱法测定方法对茶叶中的咖啡因进行检测.样品采用沸水提取,外标法定量.结果表明,在ESI正离子模式下,采用多反应监测模式进行测定时,咖啡因的检出限低,回收率高,相对标准偏差为1%~2%.
Determination of Caffeine in Tea by High Performance Liquid Chromatography-Massspectrometry
The determination of caffeine in tea by High Performance Liquid Chromatography-Mass Spectrometry was carried out.The samples were extracted by boiling water and quantified by external standard method.The results showed that the detection limit of caffeine was low,the recovery rate was high,and the relative standard deviation was 1%-2%when the multiple reaction monitoring mode was used for determination in ESI positive mode.

teacaffeineHigh Performance Liquid Chromatography-Mass Spectrometry

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福州市产品质量检验所,福建 福州 350025

茶叶 咖啡因 液相色谱串联质谱法

2024

福建分析测试
福建省测试技术研究所

福建分析测试

影响因子:0.365
ISSN:1009-8143
年,卷(期):2024.33(5)