Determination of Basic Yellow 2 in Textiles by Liquid Chromatography-Tandem Mass Spectrometry with Ultrasonic Extraction
A liquid chromatography-tandem mass spectrometry(LC-MS/MS)with ultrasonic extraction method was developed for the determination of basic yellow 2 in textiles.The textiles samples were extracted with methanol by ultrasonication,and basic yellow 2 was quantified by LC-MS/MS.The samples were detected in positive ion reaction monitoring MRM mode.A C18 column(2.1 mmX 150 mm,5 μm)was used with a gradient elution using methanol(A)-0.1％formic acid-5 mmol/L ammonium acetate aqueous solution(B)as the mobile phase.The results showed that the linearity of basic yellow 2 was good in the range of 1.0-100.0 μg/L with the R2=0.9997;the limits of detection and limits of quantification were 0.006 mg/kg and 0.02 mg/kg,respectively.The average recoveries were 82.0％-106.0％,and the relative standard deviations(RSDs)were 1.08％-7.31％(n=6).The method is suitable for the determination of basic yellow 2 in textiles.
Textilesbasic yellow 2Liquid chromatography-tandem mass spectrometryUltrasonic extraction
万方数据
维普
