首页|GC法测定复方珊瑚姜溶液尿素咪康唑软膏复合制剂中冰片的含量

GC法测定复方珊瑚姜溶液尿素咪康唑软膏复合制剂中冰片的含量

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  • NETL
  • NSTL
  • 万方数据
  • 维普
目的:建立复方珊瑚姜溶液尿素咪康唑软膏复合制剂中冰片的含量测定方法.方法:以水杨酸甲酯为内标物,PEG-20M毛细管柱、FID检测器、恒温气相色谱法测定复方珊瑚姜溶液尿素咪康唑软膏复合制剂中冰片的含量.结果:冰片在0.0401mg/mL～0.8026mg/mL范围内线性关系良好(R=0.9999),方法回收率为97.80％(RSD=0.29％).结论:方法简便,快速,准确,可用于该药品中冰片的定量测定.
GC Method for Determination of Compound Coral Miconazole Ginger Solution Urea Ointment of Borneol Content in Compound Preparation
Objectives:Establish a method to determine the borneol contents in compound coral miconazole ginger solution urea ointment.Methods:With methyl salicylic acid as the internal standard substance,determined the compound coral miconazole ginger solution urea ointment of borneol content in compound preparation PEG-20M capillary column and FID detector with constant temperature gas chromatography.Results:the borneol in 0.0401 mg/mL ～ 0.8026 mg/mL range inside have a good linear relationship (r =0.9999),recovery rate was 97.80％ (RSD =0.29％).Conclusion:The method is simple,rapid,accurate,and can be used for the quantitative determination of borneol in the drug.

borneolCompound coral miconazole ginger solution urea ointment compound preparationGCquantitative analysis

黄春青、曹桂红

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贵州省食品药品检验所,贵州贵阳550004

冰片 复方珊瑚姜溶液尿素咪康唑软膏复合制剂 GC法 含量测定

2010 ～2015年度国家药品标准提高项目

573

2016

10.16588/j.cnki.issn1002-1108.2016.04.010

贵阳中医学院学报
贵阳中医学院

贵阳中医学院学报

影响因子：1.18
ISSN：1002-1108
年,卷(期)：2016.38(4)
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