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四五老窖白酒香气成分的GC-MS分析及主要香气成分测定

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以四五老窖白酒为研究对象,采用气相色谱-质谱(GC-MS)法测定了四五老窖白酒中的香气成分,以面积归一化法测定其各组分的相对含量,共检测鉴定出45种成分,占香气总量的99.98%;同时气相色谱结合外标法测定了其中16种主要香气成分的含量,该方法线性在0.1~100 μg/mL和100~8 000 μg/mL范围内,相关系数为0.995 6~0.999 5.其中己酸乙酯(1 151.53 μg/mL,49.10%)、乳酸乙酯(769.76μg/mL,18.65%)和乙酸乙酯(430.70 μg/mL)含量较高,是该酒的主要呈香成分.
Analysis and Detection of the Mainly Aroma Components in Siwu Wine by GC-MS
The aroma scomponents in Siwulaojiao wine were analyzed by GC-MS.45 components,which up to 99.98% of total aroma components,were detected according to the peak area normalization.16 components in Siwulaojiao wine were determined quantitatively by gas chromatography with external standard method.The correlation coefficient of standard curve was 0.995 6%~0.999 5%,within a range of 0.1~100 μg/mL and 100~8 000 μg/mL of aroma components.Ethyl caproate (1 151.53 μg/mL,49.10%) and ethyl lactate(769.76 μg/mL,18.65%) were the mainly aroma components in Siwulaojiao wine.

Siwulaojiao winearomagas chromatography-mass

颜振敏、程娇娇、冯俊旗、魏新军

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河南科技学院食品学院,河南新乡 453003

四五老窖白酒 香气成分 气相色谱-质谱法

河南省科技厅科技攻关项目

132102310281

2015

湖北农业科学
湖北省农业科学院 华中农业大学 长江大学 黄冈师范学院

湖北农业科学

CSTPCD
影响因子:0.442
ISSN:0439-8114
年,卷(期):2015.54(22)
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