首页|响应面法优化超临界二氧化碳萃取法提取姜精油的工艺

响应面法优化超临界二氧化碳萃取法提取姜精油的工艺

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[目的]建立从生姜中获得高质量和高纯度姜精油的提取方法.[方法]应用超临界流体萃取技术,采取单因素和响应面优化方法,选取二氧化碳流量、姜粉过筛目数和夹带剂加入量三个因素作为考察指标,以6-姜酚得率作为姜精油提取的考察指标.[结果]通过响应面实验分析结果得到,最优姜精油提取条件为:二氧化碳流量为25 L/h,姜粉过筛目数为80目,夹带剂加入量为加入无水乙醇92.46 mL,6-姜酚的最优得率为3.21%.[结论]采用超临界二氧化碳萃取技术,通过单因素和响应面法优化实验,实现了从生姜中分离提取出高质量和高纯度姜精油的目标.
Optimization of Supercritical Carbon dioxide Extraction of Ginger Essential Oil by Response Surface Method
[Objective] Ginger essential oil (GEO) is widely used in food production and medical field in recent years due to its prominent biological functions,and this study was conducted to obtain high-quality and high-purity ginger essential oil from the fresh ginger.[Method] GEO was extracted from ginger roots by supercritical fluid extraction (SFE) method.The effects of flow rate of CO2,mesh size of ginger powder and volume of entrainer were investigated by single-factor experiments and response surface method.The content and extraction rate of 6-gingerol represented the extraction index of GEO.[Result] The conditions were optimized as follows:flow rate of CO2 at 25 L/h,mesh size of ginger power of 80 mesh,and volume of anhydrous ethanol as entrainer of 92.46 ml.The optimal extraction rate of 6-gingerol was 3.21%,which was predicted by RSM.[Conclusion] The optimal process of supercritical carbon dioxide extraction of ginger essential oil was identified by singlefactor experiments and response surface method.The present study provides a satisfactory method for purifying GEO from ginger for industrial purpose.

Ginger essential oil (GEO)Supercritical carbon dioxide extractionResponse surface methodology

雷红、周仁杰、魏巧年、李晓乐、吴静

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合肥工业大学食品科学与工程学院,安徽合肥230009

南京财经大学食品科学与工程学院,江苏南京210023

生姜精油(GEO) 超临界二氧化碳萃取法 响应面优化方法

江苏省高校自然科学研究重大项目

16KJA550001

2016

农业科学与技术(英文版)
湖南省农业科学院

农业科学与技术(英文版)

影响因子:0.222
ISSN:1009-4229
年,卷(期):2016.17(9)
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