首页|Preparation and characterization of hemihydrate calcium sulfate-calcium hydroxide composite bone repair materials

Preparation and characterization of hemihydrate calcium sulfate-calcium hydroxide composite bone repair materials

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Objective: To prepare a bone repair material with certain mechanical strength and biological activity, this paper used calcium sulfate hemihydrate (CSH) powder compounded with calcium hydroxide (Ca(OH)2) powder to prepare a bone repair scaffold material for physicochemical property characterization and testing. Methods: The physical and chemical properties and characterization of the dried and cured bone repair materials were determined by Fourier infrared spectroscopy (FT-IR), X-ray diffraction (XRD), and scanning electron microscopy;Universal material testing machine to determine the mechanical and mechanical strength of composite materials. Results: XRD showed that the structure of the composite material phase at 5% concentration was calcium sulfate hemihydrate and calcium hydroxide after hydration. The FT-IR and XRD analyses were consistent. Scanning electron microscopy (SEM) results showed that calcium hydroxide was uniformly dispersed in the hemihydrate calcium sulfate material. 0%, 1%, 5%, and 10% specimen groups had compressive strengths of 3.86±3.1, 5.27±1.28, 8.22±0.96, and 14.4±3.28 MPa. 10% addition of calcium hydroxide significantly improved the mechanical strength of the composites, but also reduced the the porosity of the material. Conclusion: With the addition of calcium hydroxide, the CSH- Ca(OH)2 composite was improved in terms of mechanical material and is expected to be a new type of bone repair material.

Calcium sulfate hemihydrateCalcium hydroxideBone defectBone repair materialCompressive strength

Zheng-Dong Guo、Yang-Yang Bian、Xiao-Qian Liu、Dong Wang、Si-Yuan Zhang、Jian Yang、Lei Peng

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Trauma medical center of the First Affiliated Hospital of Hainan Medical College,Haikou 570216,China

Key Laboratory of Emergency and Trauma Ministry of Education,Hainan Medical University,Haikou 570216,China

Key Laboratory of Hainan Trauma and Disaster Rescue,The First Affiliated Hospital of Hainan Medical University,Haikou 570216,China

国家自然科学基金Postgraduate innovation research project of Hainan Medical College

82060347HYYS2020-38

2022

海南医科大学学报(英文版)

海南医科大学学报(英文版)

ISSN:
年,卷(期):2022.28(12)
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