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毛细管气相色谱法测定六神祛暑水中樟脑与薄荷脑的含量

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建立了毛细管气相色谱同时测定六神祛暑水中樟脑、薄荷脑含量的方法.樟脑含量在0.04044 -0.505 5mg/mL范围内线性关系良好(r=0.9999),测定结果的相对标准偏差为0.79% (n=6),平均回收率为99.18%;薄荷脑含量在0.049 84-0.249 2 mg/mL范围内线性关系良好(r=0.9994),测定结果的相对标准偏差为1.5%(n=6),平均回收率为99.65%.结果表明,该定量方法精密度好,准确度高,测定简便、快速,可用于制剂的质量控制.
DETERMINATION OF CAMPHOR AND MENTHOL IN LIUSHEN QUSHU SHUI BY CAPILLARY GAS CHROMATOGRAPHY
A method for determination of camphor and menthol in Liushen Qushu Shui was established. The linear range of camphor was 0.04044 -0.5055 mg/mL with a good linear relationship(r = 0.9999) , and average recovery was 99.18% , the relative standard deviation was 0.79% ( n = 6). The linear range of menthol was 0.04984 -0.2492 mg/mL with a good linear relationship( r = 0. 9994) , and average recovery was 99.65% , the relative standard deviation was 1.5% (n = 6). This method is simple, rapid, accurate , and it can be used to control the quality of preparation.

Liushen Qushu Shui, camphor, menthol, capillary gas chromatography

温金莲、周清、唐睿、黄晓文、董宇静、黄庆华

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广东药学院药科学院,广州,510006

六神祛暑水 樟脑 薄荷脑 毛细管气相色谱法

国家自然科学基金广东省科技计划项目

810730452009198

2011

化学分析计量
中国兵器工业集团第五三研究所（国防科技工业应用化学一级计量站）

化学分析计量

CSTPCD
影响因子：0.444
ISSN：1008-6145
年,卷(期)：2011.20(5)
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