华西药学杂志2024,Vol.39Issue(6) :717-719.DOI:10.13375/j.cnki.wcjps.2024.06.017

顶空固相微萃取-GC/MS法分析四裂红景天的挥发性成分

Analysis of volatile components of Rhodiola quadrifida by HS-SPME-GC/MS

杨语 李涛 丁丹
华西药学杂志2024,Vol.39Issue(6) :717-719.DOI:10.13375/j.cnki.wcjps.2024.06.017

顶空固相微萃取-GC/MS法分析四裂红景天的挥发性成分

Analysis of volatile components of Rhodiola quadrifida by HS-SPME-GC/MS

杨语 1李涛 1丁丹1
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作者信息

  • 1. 四川大学华西药学院,四川成都 610041
  • 折叠

摘要

目的 分析鉴定四裂红景天中的挥发性成分.方法 采用顶空固相微萃取法对四裂红景天样品进行前处理,采用GC-MS法分析鉴定样品中的挥发性成分,并结合峰面积归一化法计算各组分的相对含量.结果 从四裂红景天中分析鉴定出了 75种挥发性成分,包括烷烃类、醇类、烯烃类、醛类、酸类、酮类等,各占挥发性成分总量的55.06%、13.34%、2.21%、5.53%、15.72%、6.64%.结论 四裂红景天具丰富的挥发性成分,顶空固相微萃取-GC/MS技术能便捷、准确地分析鉴别其挥发性成分.

Abstract

OBJECTIVE To analyze and identify the volatile components of Rhodiola quadrifida.METHODS The R.quadrifida sample was extracted by headspace solid phase microextraction(HS-SPME);the volatile components were analyzed and identified by gas chromatography-mass spectrometry(GC/MS);and the relative content of each compound was calculated by area normalization method.RESULTS 75 volatile components were identified from the sample of R.quadrifida,including alkanes,alcohols,olefins,aldehydes,acids,ketones,etc.They respectively accounted for 55.06%,13.34%,2.21%,5.53%,15.72%,6.64%of the volatile components.CONCLUSION The volatile components of R.quadrifida are diverse,which can be conveniently and accurately identified by HS-SPME-GC/MS.

关键词

四裂红景天/顶空固相微萃取/气相色谱/质谱/挥发性成分/成分分析

Key words

Rhodiola quadrifida/Headspace solid phase microextraction/GC/MS/Volatile components/Component analysis

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出版年

2024
华西药学杂志
四川大学,四川省药学会

华西药学杂志

CSTPCD北大核心
影响因子:0.624
ISSN:1006-0103
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