首页|一种甲氧基封端苯基甲基硅树脂预聚体合成工艺的探究

一种甲氧基封端苯基甲基硅树脂预聚体合成工艺的探究

扫码查看
以苯基三氯硅烷、二甲基二氯硅烷、甲醇、水为原料,水解缩合制备甲氧基封端的苯基甲基硅树脂预聚体.探究了水解和加料方式、溶剂、反应时间、温度等对反应过程及产物性能的影响,通过对预聚物组成、结构及性能的表征,确定了制备液体硅树脂预聚体的最优反应条件.
A Synthesis Process of Methoxy-terminated Phenyl Methyl Silicone Resin Prepolymer
A methoxy-terminated phenyl methyl silicone prepolymer was prepared by the hydrolysis-condensation reaction of phenyltrichlorosilane,dimethyldichlorosilane,methanol and water.The effects of parameters,such as hydrolysis and feeding methods,solvents,reaction time,and temperature,on reaction process and product properties were investigated.By characterizing the composition,structure,and performance of the prepolymer,the optimal reaction conditions for preparing liquid silicone resin prepolymer were determined.

methoxy-terminatedsilicone prepolymersynthesis process

王旸、杨皓、张玉霞、瞿志荣、伍川、董红

展开 >

杭州师范大学材料与化学化工学院有机硅化学及材料技术教育部重点实验室,浙江杭州311121

氟硅精细化学品与材料制造协同创新中心,浙江杭州311121

甲氧基封端 硅树脂预聚体 合成工艺

浙江省公益计划资助项目

LGG21B040002

2024

杭州师范大学学报(自然科学版)
杭州师范大学

杭州师范大学学报(自然科学版)

CSTPCD
影响因子:0.386
ISSN:1674-232X
年,卷(期):2024.23(3)
  • 5