首页|基于DoE实验设计的硝酸铈溶液雾化特性研究

基于DoE实验设计的硝酸铈溶液雾化特性研究

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为满足喷雾热分解法制备氧化铈颗粒需求,使用两相流空气辅助雾化喷嘴,对不同浓度的硝酸铈溶液雾化特性进行了实验研究,并使用响应曲面法对硝酸铈溶液喷雾的雾化颗粒度SMD实验数据进行了定量分析,得到了雾化颗粒度SMD与溶液物理性质及雾化环境参数之间的定量关系.本实验中溶液质量浓度为0.334~0.462、溶液体积流量为0.05 m3/h和0.12 m3/h、雾化空气压力为0.2~0.5 MPa.根据对获得的定量关系式分析可知,对硝酸铈溶液雾化颗粒度SMD影响最显著的因素是溶液浓度,其次是雾化空气压力,溶液体积流量对雾化颗粒度SMD的影响较小;雾化颗粒度均随雾化空气压力的升高而减小,雾化空气压力对粘性较小溶液的影响更加显著.
Research on the Atomization Characteristics of Cerium Nitrate Solution based on Design of Experiment
In order to meet the requirements of the spray pyrolysis method for preparing cerium oxide par-ticles,the atomization characteristics of cerium nitrate solution with different concentrations were studied experimentally by using a two-phase flow air-assisted atomization nozzles,and the atomization particle size SMD experimental data of cerium nitrate solution spray were quantitatively analyzed by response sur-face method and the quantitative relationship between atomization particle size SMD and solution physical properties and atomization environment parameters was obtained.In this experiment,the mass concentra-tion of the solution is 0.334~0.462,the volume flow rate of the solution is 0.05 m3/h and 0.12 m3/h,and the atomization air pressure is 0.2~0.5 MPa.According to the quantitative relationship analysis,the most significant factor affecting the atomization particle size SMD of cerium nitrate solution is the solu-tion concentration,followed by the atomization air pressure,and the solution volume flow rate has little effect on the atomization particle size SMD;the atomization particle size decreases with the increase of at-omization air pressure,and the effect of atomization air pressure on the less viscous solution is more sig-nificant.

cerium nitrate solutionatomized particle size SMDatomization characteristicsdesign of experimentresponse surface method

薛炜宸、陈静、霍伟业、侯蕾、陈杨

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北华航天工业学院 航空宇航学院,河北 廊坊 065000

中国核电工程有限公司,北京 100191

中国人民解放军95866 部队,河北 保定 071100

硝酸铈溶液 雾化颗粒度SMD 雾化特性 DoE实验设计 响应曲面法RSM

北华航天工业学院博士科研启动基金北华航天工业学院硕士研究生创新项目

BKY202110YKY-2022-44

2024

节能技术
国防科技工业节能技术服务中心

节能技术

CSTPCD
影响因子:0.601
ISSN:1002-6339
年,卷(期):2024.42(1)
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