金属热处理2024,Vol.49Issue(12) :57-61.DOI:10.13251/j.issn.0254-6051.2024.12.009

退火温度对NdFeB磁体微观结构与磁性能的影响

Effect of annealing temperature on microstructure and magnetic properties of NdFeB magnets

李欢 王俊勃 刘江南 思芳 吴树杰 董义
金属热处理2024,Vol.49Issue(12) :57-61.DOI:10.13251/j.issn.0254-6051.2024.12.009

退火温度对NdFeB磁体微观结构与磁性能的影响

Effect of annealing temperature on microstructure and magnetic properties of NdFeB magnets

李欢 1王俊勃 2刘江南 2思芳 2吴树杰 3董义3
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作者信息

  • 1. 西安摩尔石油工程实验室股份有限公司,陕西西安 710065;西安工程大学材料工程学院,陕西西安 710048
  • 2. 西安工程大学材料工程学院,陕西西安 710048
  • 3. 包头天和磁材科技股份有限公司,内蒙古包头 014010
  • 折叠

摘要

为研究退火处理对钕铁硼磁体微观结构和磁性能的影响,对粉末烧结钕铁硼磁体在500-600℃下进行退火处理,采用XRD、SEM、磁性能测量仪对NdFeB磁体进行分析与表征.结果表明,退火处理对NdFeB磁体主相Nd2Fe14B的结构影响很小,主要是影响富Nd相的分布与成分.退火处理后NdFeB磁体的内禀矫顽力都有不同程度的提升.经550℃退火处理后,富Nd相连续、均匀分布于主相Nd2Fe14B晶粒边界,且富Nd相中Nd的含量增加,Fe的含量降低,磁体的内禀矫顽力提升效果最佳,从1135 kA/m提高到1434 kA/m,相应提升了 26.3%;退火处理后磁体的剩磁没有明显变化,最大磁能积有不同程度的降低.

Abstract

To investigate the effect of annealing treatment on the microstructure and magnetic properties of NdFeB magnets,powder sintered NdFeB magnets were annealed at 500-600 ℃.XRD,SEM and magnetic performance measuring instruments were used to analyze and characterize the NdFeB magnets.The results show that the annealing treatment has little effect on the structure of the main phase Nd2Fe14B of the NdFeB magnets,but mainly affects the distribution and composition of the rich-Nd phase.After annealing treatment,the coercivity of the NdFeB magnets is improved to varying degrees.After annealing at 550 ℃,the rich Nd phase is continuous and uniformly distributed along the grain boundaries of the Nd2Fe14B main phase,and the content of Nd in the rich-Nd phase increases while the content of Fe decreases,and the coercivity of the magnets has the best improvement effect,increasing from 1135 kA/m to 1434 kA/m,correspondingly increased by 26.3%.After annealing treatment,the residual magnetism of the magnets doesn't change significantly,but the maximum magnetic energy product decreases to varying degrees.

关键词

钕铁硼磁体/退火温度/微观结构/内禀矫顽力/剩磁/最大磁能积

Key words

NdFeB magnets/annealing temperature/microstructure/coercivity/residual magnetism/maximum magnetic energy product

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出版年

2024
金属热处理
北京机电研究所 中国机械工程学会热处理学会 中国热处理行业协会

金属热处理

CSTPCDCSCD北大核心
影响因子:0.546
ISSN:0254-6051
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