首页|真空碳热还原ITO废靶回收金属铟的工艺研究

真空碳热还原ITO废靶回收金属铟的工艺研究

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以ITO(Indium-Tin-Oxide)废靶为原料进行一步真空碳热还原蒸馏回收金属铟的实验.首先研究了碳热还原过程中温度、保温时间、碳粉添加量对铟还原率的影响,再结合铟锡合金的真空蒸馏进行ITO废靶的一步还原蒸馏回收金属铟.最佳真空碳热还原条件:温度900℃,保温时间2h,真空度10~20 Pa,碳粉添加量为质量分数16%.一步还原蒸馏最佳条件:温度900℃,保温时间2h,碳粉添加量为质量分数16%.真空度10~20 Pa的条件下充分还原后,再进行真空蒸馏:温度1 200℃,保温时间1h,真空度10~20 Pa.可通过一步真空碳热还原蒸馏实现从ITO废靶中直接回收金属铟.
Process Study on Vacuum Carbon Thermal Reduction for the Recovery of Indium Metal from ITO Waste Targets
Experimental study was conducted on the one-step vacuum carbon thermal reduction distillation for the recovery of indium metal from Indium-Tin-Oxide(ITO)waste targets.The influence of temperature,insu-lation time,and carbon powder addition on the indium reduction rate during the carbon thermal reduction process was investigated.Additionally,the one-step reduction distillation recovery of indium metal from ITO waste tar-gets was studied in conjunction with the vacuum distillation of indium-tin alloy.The optimal conditions for vacu-um carbon thermal reduction were determined as follows:temperature of 900℃,insulation time of 2 hours,vacu-um degree of 10-20 Pa,and carbon powder addition of 16%(mass fraction).The optimal conditions for one-step reduction distillation were found to be a temperature of 900℃,insulation time of 2 hours,and carbon powder addition of 16%(mass fraction).After sufficient reduction under conditions of 10-20 Pa vacuum degree,vacu-um distillation was then performed at a temperature of 1 200℃,insulation time of 1 hour,and vacuum degree of 10-20 Pa.Direct recovery of indium metal from ITO waste targets was achieved through the one-step vacuum carbon thermal reduction distillation process.

ITO waste targetindiumvacuum carbothermal reductionIndium-Tin separation

王红玉、邓勇、赵玺然、杜巧圆

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昆明理工大学 冶金与能源工程学院,云南 昆明 650093

ITO废靶 金属铟 真空碳热还原 铟锡分离

兴滇英才支持计划青年人才专项

2024

昆明理工大学学报(自然科学版)
昆明理工大学

昆明理工大学学报(自然科学版)

CSTPCD北大核心
影响因子:0.516
ISSN:1007-855X
年,卷(期):2024.49(1)
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