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电感耦合等离子体质谱法测定可降解餐盒中铅的不确定度评定

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本文对可降解餐盒中铅含量进行测定,探索影响可降解餐盒中铅检测结果测量不确定度的主要因素及降低不确定度的具体方法.结果表明,植物基可降解餐盒中铅的含量为 0.75 mg·kg-1,扩展不确定度为0.03 mg·kg-1,测定结果表示为(0.75±0.03)mg·kg-1,k=2.影响测定结果可靠性的主要因素是拟合曲线引入的不确定度,其次是样品重复性测量、标准系列溶液配制、样品称量和消解过程中引入的不确定度,样品消解液定容引入的不确定度可忽略不计.
Evaluation of Uncertainty in the Determination of Lead in Degradable Meal Boxes by Inductively Coupled Plasma Mass Spectrometry
This article determines the lead content in biodegradable food boxes,explores the main reasons that affect the measurement uncertainty of lead detection results in biodegradable food boxes,and specific methods to reduce uncertainty.The results showed that the lead content in plant-based biodegradable food boxes was 0.75 mg·kg-1,with an expanded uncertainty of 0.03 mg·kg-1.The measurement result was expressed as(0.75±0.03)mg·kg-1,k=2.The main factor affecting the reliability of measurement results is the uncertainty introduced by the fitting curve,followed by the uncertainty introduced during sample repeatability measurement,standard series solution preparation,sample weighing,and digestion process.The uncertainty introduced by the constant volume of sample digestion solution can be ignored.

degradable packing meal boxeleadinductively coupled plasma mass spectrometryuncertainty

董丹丹、马玉婷、牛记者、王斌、戴婕妤、王莲芳、叶峰

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杭州市余杭区食品药品监测中心,浙江 杭州 311199

可降解餐盒 电感耦合等离子体质谱法 不确定度

浙江省市场监督管理局雏鹰计划培育项目

CY2023317

2024

现代食品
国家粮食储备局郑州科学研究设计院

现代食品

影响因子:0.169
ISSN:2096-5060
年,卷(期):2024.30(1)
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