Determination of 2 Sweeteners in Grape by UPLC-MS/MS
Establishing a method for the qualitative analysis and quantitative detection of sweeteners such as sodium cyclamate and neotame in grape samples using a ultra high performance liquid chromatography triple quadrupole mass spectrometer system.The samples are prepared and injected into the instrument after extraction,utilizing a multiple reaction monitoring mode and negative ion scanning.There is a good linear relationship in 1～50 ng·mL-1,with a spike recovery rate of 87.6%to 96.8%and the relative standard deviation≤5.8%.This method is characterized by its simplicity in sample preparation,high detection efficiency,accuracy,and good repeatability.It can be used for the detection of certain sweeteners in fresh grape samples.
sodium cyclamateneotamegrapeultra high performance liquid chromatography triple quadrupole mass spectrometer
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