Determination of 1-Decene Migrated from Plastic Products for Food Contact by Gas Chromatography Mass Spectrometry
A gas chromatography-mass spectrometry analysis method for 1-decene has been established to provide a methodological basis for the detection of 1-decene migration in plastic products for food contact.In the migration experiment,n-hexane was selected as the food simulant,the migration temperature was set to 60℃,the migration time was 2 h,and the migration test solution was detected by gas chromatography-mass spectrometer.The results showed that the target analytes showed good linearity in the concentration range of 5～100 µg·L-1 with the linear correlation coefficient(R2)of 0.999 6.The limit of quantification was 0.005 mg·kg-1,and the recoveries were in the range of 87.4%～106.0%with the relative standard deviations of 2.1%～3.4%.The method is fast,accurate,and highly sensitive,and is available for the detection of 1-decene migration in plastic products for food contact.
plastic products for food contact1-decenemigration quantitygas chromatography-mass spectrometry
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