现代食品2024,Vol.30Issue(10) :167-173.DOI:10.16736/j.cnki.cn41-1434/ts.2024.10.052

基于OAV和GC-O-MS法表征丁香花蕾油关键香气成分

Identification of the key Aroma Components in Clove Bud Essential Oil using OVA and GC-O-MS

赵新玉 申思 毛华 孙泽平 齐海楠 叶秋明 袁子豪 王存喜
现代食品2024,Vol.30Issue(10) :167-173.DOI:10.16736/j.cnki.cn41-1434/ts.2024.10.052

基于OAV和GC-O-MS法表征丁香花蕾油关键香气成分

Identification of the key Aroma Components in Clove Bud Essential Oil using OVA and GC-O-MS

赵新玉 1申思 1毛华 1孙泽平 1齐海楠 1叶秋明 1袁子豪 1王存喜1
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作者信息

  • 1. 红塔辽宁烟草有限责任公司,辽宁 沈阳 110001
  • 折叠

摘要

为了表征丁香花蕾油关键香气成分,本研究利用香气活度值(OAV)和气相色谱-嗅闻-质谱联用技术(GC-O-MS)进行分析鉴定.GC-O-MS分析鉴定丁香花蕾油含有 59 种挥发性成分.通过嗅闻强度计算确定 2-甲基丁酸乙酯、2-壬酮、芳樟醇、水杨酸甲酯、对烯丙苯酚、肉桂酸乙酯和丁香酚 7 种香气活性成分.经OAV计算,确定芳樟醇、2-甲基丁酸乙酯、乙酸苏合香酯、水杨酸甲酯、肉桂酸乙酯、丁香酚、对烯丙苯酚、α-葎草烯和石竹素9种香气成分,通过两种分析手段共同鉴定出的丁香酚、2-甲基丁酸乙酯、芳樟醇、水杨酸甲酯、对烯丙苯酚和肉桂酸乙酯为丁香花蕾油的关键香气成分.

Abstract

In order to characterize the key aroma components of clove bud oil,aroma activity value(OAV)and gas chromatography-odor-mass spectrometry(GC-O-MS)were used in this study.GC-O-MS analysis identified 59 volatile components in clove bud oil.7 aroma active ingredients,including ethyl 2-methylbutyrate,2-nonone,linalool,methyl salicylate,p-allylphenol,ethyl cinnamate and eugenol,were determined by odor intensity calculation.Nine aroma components,linalool,ethyl 2-methylbutyrate,tholyl acetate,methyl salicylate,ethyl cinnamate,eugenol,p-allylphenol,α-humulene and caryophyllene,were identified by OAV calculation.Eugenol,ethyl 2-methylbutyrate,linalool,methyl salicylate,p-allylphenol and ethyl cinnamate were identified as lilac flower buds by two analytical methods Key aroma component of oil.

关键词

丁香花蕾油/气相-质谱-嗅闻仪(GC-O-MS)/香气活力值(OAV)/关键香气成分

Key words

clove bud essential oil/gas chromatography olfactory mass spectrometry(GC-O-MS)/odor activity value(OAV)/key aroma components

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基金项目

中国烟草实业发展中心科技项目(ZYSYQ-2023-05)

出版年

2024
现代食品
国家粮食储备局郑州科学研究设计院

现代食品

影响因子:0.169
ISSN:2096-5060
参考文献量10
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