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QuEChERS前处理法测定茶叶中8种农药残留

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本研究采用QuEChERS法测定茶叶中8种农药残留量.茶叶样品中的氧乐果、吡虫啉、啶虫脒、灭多威、克百威、3﹣羟基克百威、异丙威、氯虫苯甲酰胺残留经乙腈提取,以QuEChERS散化固相萃取小柱吸附提取液中的有机酸、色素等杂质,再经离心、过滤后经UPLC-MS/MS法测定,外标基质法定量,研究提取、净化的最优条件.
Determination of Eight Pesticide Residues in Tea by QuEChERS Pretreatment Method
The QuEChERS method was used to determine eight pesticide residues in tea.The residues of omethoate,imidacloprid,diniprid,Metocarb,carboxanil,3-hydroxycarboxanil,isoprocarb and chlorobenzamide in tea samples were extracted by acetonitrile.Organic acids,pigments and other impurities were adsorbed by QuEChERS dispersive solid phase extraction column,then determined by UPLC-MS/MS method after centrifugation and filtration,and quantified by external standard matrix method.The optimum conditions for extraction and purification were studied.

QuEChERSUPLC-MS/MSteadeterminationpesticide residues

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名成腾德检测服务(福州)有限公司,福建 福州 350007

QuEChERS UPLC-MS/MS 茶叶 测定 农药残留

2024

现代食品
国家粮食储备局郑州科学研究设计院

现代食品

影响因子:0.169
ISSN:2096-5060
年,卷(期):2024.30(18)