首页|溶胶温度、冷却温度对κ-卡拉胶凝胶微观形貌的影响

溶胶温度、冷却温度对κ-卡拉胶凝胶微观形貌的影响

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目的:研究溶胶温度、冷却温度对κ-卡拉胶微观形貌的影响,为实现加热型凝胶工艺的精准控制提供参考.方法:采用扫描电子显微镜对在不同溶胶温度与冷却温度下制备κ-卡拉胶凝胶进行形貌表征.结果:在80℃水浴温度下溶胶,随着冷却温度的降低,凝胶结构由无序堆叠形态向有序三维网状结构转变;温差过大时,凝胶微观结构易产生丝状物牵连.采用自然冷却工艺凝胶时,溶胶温度越高,凝胶三维网状结构越明显.在100℃水浴温度下溶胶,冷却温度对凝胶微观结构基本无影响.在 90℃及以下水浴温度溶胶,凝胶受冷冻影响较大且会产生明显塌缩,不利于还原真实的凝胶形貌.结论:溶胶温度与冷却温度对κ-卡拉胶凝胶的微观形貌有明显影响.
Effects of Sol Temperature and Cooling Temperature on the Micro Morphology of κ-Carrageenan
Objective:To study the influence of sol temperature and cooling temperature on the micro morphology of κ-carrageenan,and to provide reference for the precise control of heated gel process.Method:Scanning electron microscope was used to characterize the morphology of κ-carrageenan gel prepared at different sol temperatures and cooling temperatures.Result:At the water bath temperature of 80℃,the structure of gel changed from disordered stacking to ordered three-dimensional network structure with the decrease of cooling temperature.When the temperature difference is too large,the microstructure of gel is easy to produce filaments.When gel is naturally cooled,the higher the sol temperature is,the more obvious the three-dimensional network structure of gel is.At 100℃water bath temperature,the cooling temperature of sol has little effect on the microstructure of gel.At water bath temperature of 90℃and below,the gel is greatly affected by freezing and will produce obvious collapse,which is not conducive to restoring the true gel morphology.Conclusion:The sol temperature and cooling temperature have obvious influence on the micro morphology of κ-carrageenan.

gelscanning electron microscopecarrageenansol temperaturecooling temperature

邓甜甜、王婧、吴志伟

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深圳波顿香料有限公司 新材研发部,广东 深圳 518000

波顿(湖北)生物科技有限公司 研发部,湖北 仙桃 433000

凝胶 扫描电镜 卡拉胶 溶胶温度 冷却温度

2024

现代食品
国家粮食储备局郑州科学研究设计院

现代食品

影响因子:0.169
ISSN:2096-5060
年,卷(期):2024.30(19)