Determination of Migration Residual Value of Dibutyl Phthalate in Peanut Oil by Triple Quadrupole Gas Chromatography-Mass Spectrometry
This article establishes a detection method for the migration residue of dibutyl phthalate(DBP)in peanut oil using triple quadrupole gas chromatography-mass spectrometry.The results showed that DBP had a good linear relationship between 25～1 000 μg·L-1,with a correlation coefficient of 0.999 4;the detection limit of the method is 0.02 μg·kg-1,and the quantification limit is 0.06 μg·kg-1;when the spiked concentration is 20～60 μg·kg-1,the recovery rate is 91.72%～103.30%,and the relative standard deviation is 7.565%～9.886%.This method has simple and efficient preprocessing,high sensitivity,and good specificity,which can meet the daily detection and analysis of DBP migration residue values in peanut oil.
triple quadrupole gas chromatographdibutyl phthalatesolid phase extractionpeanut oil
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NSTL
万方数据
维普
