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三勒浆饮品中柯里拉京测定方法研究

Research on the Determination Method of Corilagin in Sanajon Beverage

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采用HPLC法构建三勒浆饮品中柯里拉京的测定方法.采用C18色谱柱(150 mm,5 μm),乙腈-0.5%醋酸(1∶9)为流动相,流速1.0 mL·min-1,柱温30℃,检测波长272 nm.结果显示,柯里拉京在0.114~1.14 μg范围内线性关系良好,平均加样回收率为101.5%,RSD为1.5%.6批样品中柯里拉京的含量分别为83、80、81、70、78、74 mg/100 mL.该测定方法重现性好、精确度高、简便易行,可以为三勒浆饮品的质量控制提供可靠依据.
HPLC method was developed for the determination of corilagin in sanajon beverage.The determination was performed on a C18 column(150 mm,5 μm)with acetonitrile-0.5%acetic acid(1∶9)as the mobile phase at the flow rate of 1.0 mL·min-1.The column temperature was 30℃and the detection wavelength was 272 nm.The results showed that corilagin had a good linear relationship in the range of 0.114~1.14 μg.The average recovery was 101.5%and RSD was 1.5%.The contents of corilagin in 6 batches of samples were 83,80,81,70,78,74 mg/100 mL,respectively.The method has good reproducibility,high accuracy and simplicity,and can provide a reliable basis for the quality control of sanajon beverage.

corilagindetermination methodHPLC

黄辉、莫太刚、代庆、孟伦秀、马彬伦、李桂晖、段兰兰

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成都三勒浆药业集团四川华美制药有限公司,四川 成都 610045

柯里拉京 测定方法 HPLC

2024

现代食品
国家粮食储备局郑州科学研究设计院

现代食品

影响因子:0.169
ISSN:2096-5060
年,卷(期):2024.30(20)