毛纺科技2024,Vol.52Issue(5) :103-107.DOI:10.19333/j.mfkj.20231103805

铜氨溶液法定量分析蚕丝/羊毛混合物

Quantitative analysis of silk/wool mixture by copper ammonia solution

肖传志 徐杰 马国阳 余晓筠 陈忆霞 杨清
毛纺科技2024,Vol.52Issue(5) :103-107.DOI:10.19333/j.mfkj.20231103805

铜氨溶液法定量分析蚕丝/羊毛混合物

Quantitative analysis of silk/wool mixture by copper ammonia solution

肖传志 1徐杰 1马国阳 1余晓筠 1陈忆霞 1杨清1
扫码查看

作者信息

  • 1. 广东省江门市质量计量监督检测所,广东 江门 529000
  • 折叠

摘要

为了准确测定蚕丝/羊毛混合物中纤维含量,选用铜氨溶液试剂定量分析蚕丝/羊毛混合物.选择试验温度、振荡频率、振荡时间为试验因素,羊毛含量测试值与实际值的绝对差值为试验指标,首先采用单因素试验法确定各试验因素的较优范围,然后在较优范围内选择各试验因素进行三水平正交试验,通过对试验数据的分析得到最优试验条件,最后使用最优试验条件测试纯羊毛织物,计算得到羊毛的修正系数.结果表明:铜氨溶液法定量分析蚕丝/羊毛混合物的最优试验条件为试验温度 40℃、振荡频率 150 r/min、振荡时间 40 min;羊毛的修正系数(d值)为 0.998 9,该方法操作简便,结果准确,重复性好.

Abstract

In order to accurately determine the fiber content of silk/wool mixture,copper ammonia solution reagent was used to quantitatively analyze silk/wool mixture.The test temperature,oscillation frequency and oscillation time were selected as the test factors,and the absolute difference between the test value and the actual value of wool content was selected as the test index.Firstly,the single factor test method was used to determine the optimal range of each test factor.Then,each test factor was selected within the optimal range to carry out three-level orthogonal test.The optimal test conditions were obtained by analyzing the test data.Finally,the pure wool fabric was tested under the optimal test conditions,and the correction coefficient of wool was calculated.The results show that the optimal test conditions for quantitative analysis of silk/wool mixture by copper ammonia solution are as follows:test temperature 40℃,oscillation frequency 150 r/min,oscillation time 40 min;the correction coefficient of wool(d value)is 0.998 9.The method is simple,accurate and reproducible.

关键词

蚕丝/羊毛/混合物/定量分析/铜氨溶液

Key words

silk/wool/mixture/quantitative analysis/copper ammonia solution

引用本文复制引用

出版年

2024
毛纺科技
中国纺织信息中心 北京毛纺织科学研究所

毛纺科技

北大核心
影响因子:0.3
ISSN:1003-1456
参考文献量10
段落导航相关论文