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煤中氟和氯含量的检测方法研究

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阐述了煤中氟和氯元素对生态环境的危害,试验测试了天水市域内煤中氟、氯元素含量范围,氟含量分布区间为20~197 μg/g,氯含量分布区间为0.003%~0.139%.同时,研究发现,高温燃烧水解—离子色谱法适用于煤炭中氟和氯的快速检测,适用于实验室日常检验检测.
Study on the determination method of fluorine and chlorine in coal
In this paper,the hazards and content range of fluorine and chlorine in coal are discussed.the distribution range of fluorine content in Tianshui City is 20pg/g~197μg/g.The chlorine content ranges from 0.003%to 0.139%.At the same time,the pretreatment method and measurement method of fluorine and chlorine were studied.Finally,it was found that the high temperature combustion hydrolyzation-ion chromatography method is suitable for the rapid detection of fluorine and chlorine in coal.Compared with the international standard,this method has high sensitivity,good repeatability and reproducibility,it can rapidly detect fluorine and chlorine in coal at the same time,which can greatly improve the detection efficiency.Suitable for daily laboratory inspection and testing.

coalfluorine contentchlorine contenthigh temperature hydrolysision chromatography

杨丽娟、宋高林

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甘肃省产品质量监督检验东部分中心,甘肃天水 741000

煤炭 氟含量 氯含量 高温水解 离子色谱

甘肃省市场监督管理局科技计划项目

SSCJG-ZJ-A202207

2024

煤炭加工与综合利用
中国煤炭加工利用协会

煤炭加工与综合利用

影响因子:0.496
ISSN:1005-8397
年,卷(期):2024.(1)
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