热加工工艺2024,Vol.53Issue(14) :69-72.DOI:10.14158/j.cnki.1001-3814.20212152

CNTs/Cu层状复合材料的制备及其组织和性能研究

Research on Preparation of CNTs/Cu Layered Composite and Its Microstructure and Properties

徐雪霞 王勇 李文彬 董国振 李国维 刘洹钰 丁海民
热加工工艺2024,Vol.53Issue(14) :69-72.DOI:10.14158/j.cnki.1001-3814.20212152

CNTs/Cu层状复合材料的制备及其组织和性能研究

Research on Preparation of CNTs/Cu Layered Composite and Its Microstructure and Properties

徐雪霞 1王勇 1李文彬 1董国振 1李国维 1刘洹钰 2丁海民2
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作者信息

  • 1. 国网河北省电力有限公司电力科学研究院,河北 石家庄 050021;国网河北能源技术服务有限公司,河北 石家庄 050021
  • 2. 华北电力大学 能源动力与机械工程学院,河北 保定 071003
  • 折叠

摘要

采用扩散结合法将分散后的碳纳米管附着在铜箔表面,经裁剪、堆叠和预压后使用真空热压烧结炉进行烧结,制备出具有优良导电性的CNTs/Cu层状复合材料.使用SEM、EDS和XRD等对样品的微观形貌和成分进行表征,使用显微硬度计和导电率检测仪等对样品性能进行测试.结果表明:在热压烧结过程中,一定量铜扩散到CNTs层中,有效改善了碳纳米管层和铜层的结合能力.相比于纯铜,CNTs/Cu层状复合材料在硬度提高 45%的同时,在平行于碳纳米管层方向导电率达到 91%IACS,而垂直于碳纳米管层方向也仍具有 80.6%IACS的导电率.

Abstract

The dispersed carbon nanotubes were attached to the surface of copper foil by diffusion bonding method.After cutting,stacking and pre-pressing,CNTs/Cu layered composite with excellent conductivity were prepared by sintering in vacuum hot pressing sintering furnace.The microscopic characterization of CNTs/Cu layered composite was carried out by SEM,EDS and XRD.Sample performance was tested using a microhardness meter and a conductivity detector,etc.The results show that during hot pressing sintering,a certain amount of copper diffuses into CNTs layer,which effectively improves the bonding ability between CNTs layer and copper layer.Compared with pure copper,CNTs/Cu layered composite not only improve the hardness by 45%,but also achieve 91%IACS in the direction parallel to the carbon nanotube layer and 80.6%IACS in the direction perpendicular to the carbon nanotube layer.

关键词

碳纳米管/扩散结合法/CNTs/Cu复合材料/导电性

Key words

carbon nano-tubes(CNTs)/diffusion bonding method/CNTs/Cu composite/conductivity

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基金项目

国网河北能源技术服务有限公司项目(TSS2020-10)

出版年

2024
热加工工艺
中国船舶重工集团公司热加工工艺研究所 中国造船工程学会船舶材料学术委员会

热加工工艺

CSTPCD北大核心
影响因子:0.55
ISSN:1001-3814
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