首页|参芪复合固体饮料中3种有效成分检测方法的建立及其含量稳定性的研究

参芪复合固体饮料中3种有效成分检测方法的建立及其含量稳定性的研究

扫码查看
通过HPLC测定参芪复合固体饮料中人参皂苷Rg1、甘草酸、黄芪甲苷的含量,并进行加速试验考察其稳定性.结果表明,人参皂苷Rg1、甘草酸、黄芪甲苷分别在3.1709~63.4186 μg/mL、0.7945~15.8993 μg/mL、20.3199~203.1993 μg/mL浓度范围内线性良好,加标回收率范围分别为100.27%~104.87%、100.74%~104.72%、103.07%~107.54%.在3个月加速试验中,该固体饮料性状、感官、溶解度均符合要求;3种成分含量均呈现出良好的稳定性.表明参芪复合固体饮料中人参皂苷Rg1、甘草酸、黄芪甲苷的含量在3个月加速试验中相对稳定,该研究可为参芪复合固体饮料的有效期制定提供良好依据.
Study on the Establishment of Detection Methods and Content Stability of Three Effective Components in Shenqi Compound Solid Beverage
HPLC was used to determine the content of ginsenoside Rg1,glycyrrhizic acid,and astragaloside Ⅳ in Shenqi compound solid beverage,and their stability was investigated through accelerated experiment.The results showed that ginsenoside Rg1,glycyrrhizic acid,and astragaloside Ⅳ had a good linear relation in the respective concentration range of 3.1709~63.4186 μg/mL,0.7945~15.8993 μg/mL and 20.3199~203.1993 μg/mL,the range of sample recovery rates were 100.27%~104.87%,100.74%~104.72%,103.07%~107.54%,respectively.3-month accelerated experiment showed that textural properties,sensory properties,and solubility of the solid beverage met the requirements;The content of all three components showed good stability.This indicates the stability of ginsenoside Rg1,glycyrrhizic acid,and astragaloside Ⅳ in Shenqi compound solid beverage was good in 3-month accelerated experiment,this study provides a good reference for determining the expiration date of Shenqi compound solid beverage.

solid beverageginsenoside Rg1glycyrrhizic acidastragaloside ⅣstabilitiesHPLC

黄盼、曹菁、王忠稳、郝江伟、王晨

展开 >

劲牌持正堂药业有限公司,黄石 435000

中药保健食品与安全湖北省重点实验室,大冶 435100

固体饮料 人参皂Rg1 甘草酸 黄芪甲苷 稳定性 高效液相色谱

湖北省科技重大专项课题

2020ACA007

2024

食品与发酵科技
四川省食品发酵工业研究设计院

食品与发酵科技

CSTPCD
影响因子:0.508
ISSN:1674-506X
年,卷(期):2024.60(5)