山东化工2024,Vol.53Issue(4) :55-61.

2,2'-联吡啶的合成研究

Study on the Synthesis of 2,2'-Bipyridine

王文魁 丁永山 岳瑞宽 陈洪龙 罗超然
山东化工2024,Vol.53Issue(4) :55-61.

2,2'-联吡啶的合成研究

Study on the Synthesis of 2,2'-Bipyridine

王文魁 1丁永山 1岳瑞宽 1陈洪龙 1罗超然1
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作者信息

  • 1. 南京红太阳生物化学有限公司,江苏南京 210047
  • 折叠

摘要

以吡啶为原料,采用催化剂催化偶联合成2,2'-联吡啶,收率达到81%,探索了温度、压力、反应器、原料等对催化剂寿命及产能的影响.同时,研究了不同条件下,副产物哌啶的生成量,探究了吡啶哌啶分离方法.

Abstract

Bipyridine was synthesized from pyridine under the catalyst,the yied was 66%.The effects of temperature,pressure,catalyst,reactor and raw materials on the yield of bipyridine were investigated.At the same time,the production amount of byproduct piperidine under different conditions was studied,and the separation method of pyridine piperidine was explored.

关键词

敌草快/联吡啶/哌啶/固定床反应器/负载镍

Key words

diquat/bipyridine/piperidine/fixed bed reactor/loaded nickel

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出版年

2024
山东化工
山东省化工研究院 山东省化工信息中心

山东化工

影响因子:0.249
ISSN:1008-021X
参考文献量3
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