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ICP-MS法测定鹿骨胶中铝残留量

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目的:建立鹿骨胶中铝残留量的测定方法。方法:采用电感耦合等离子体质谱法(ICP-MS)测定鹿骨胶中铝的残留量。结果:鹿骨胶中铝的测定值在相应的线性范围内,线性关系良好,精密度、准确度、耐用性试验中铝残留浓度相对标准偏差均小于 3。0%,平均加样回收率为99。6%(Sc内标)/103。8%(Ge内标),且相对标准偏差分别为0。6%/1。0%。结论:该方法具有良好的专属性和重现性,加样回收率符合要求,结果准确且稳定,适用于测定鹿骨胶中铝残留含量。
Determination of Aluminum Residue in Deer Bone Glue by ICP-MS Method
Objective:To establish a method for the determination of residual aluminum in deer bone glue.Methods:The residual content of aluminum in deer bone glue was determined by inductively coupled plasma mass spectrometry(ICP-MS).Results:The determination values of aluminum in deer bone glue were in the corresponding linear range,and the linear relationship was good.The relative standard deviation of aluminum residual concentration in precision,accuracy and durability tests was less than 3.0%,the average recovery rate was 99.6%(Sc internal standard)/103.8%(Ge internal standard),and the relative standard deviation was 0.6%/1.0%,respectively.Conclusion:The method has good specificity and reproducibility,the recovery rate meets the requirements,the results are accurate and stable,and it is suitable for the determination of residual content of aluminum in deer bone glue.

deer bone gluealuminuminductively coupled plasma mass spectrometry

余彩娟、刘册家、林超、高习宸、孙珊珊、于春芳

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山东中医药大学药学院,山东济南 250100

山东宏济堂制药集团股份有限公司,山东济南 250103

山东大学药学院,山东济南 250012

济南市食品药品检验检测中心,山东济南 250103

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鹿骨胶 电感耦合等离子体质谱法

2024

山东化工
山东省化工研究院 山东省化工信息中心

山东化工

影响因子:0.249
ISSN:1008-021X
年,卷(期):2024.53(5)
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