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固相光度法测定樟树树叶中微量稀土元素含量研究

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以石蜡为固体萃取剂,8-羟基喹啉为显色剂,采用固相光度法测定樟树树叶中微量稀土元素的含量,探讨了不同因素对稀土元素测定的影响,确定了最佳分析条件。当镧稀土元素的质量浓度为0~1。6 μg/mL时,溶液褪色程度与镧稀土元素含量呈线性关系,符合朗伯-比尔定律。镧稀土元素测试的相对标准偏差为2。5%,加标回收率为 94。3%~106。1%。本方法灵敏度高、选择性好,测试结果满意。
Determination of Trace Rare Earth Element Content in Camphor Tree Leaves by Solid-phase Spectrophotometry Research
Trace rare earth elements in camphor tree leaves was determined by solid-phase spectrophotometry with paraffin as a solid extraction agent and 8-hydroxyquinoline as a chromogenic agent.The influence was investigated of various factors on rare earth elements and the optimum analytical conditions were determined.When the mass concentration of lanthanide rare earth elements ranges from 0 to 1.6 μg/mL,there is a linear relationship between color fading degree and lanthanide rare earth elements content following Beer's law.The relative standard deviation for the testing of lanthanide rare earth elements is 2.5%,and the spike recovery rate ranges from 94.3%to 106.1%.This method exhibits high sensitivity,excellent selectivity,and satisfactory test results.

paraffin8-hydroxyquinolinesolid-phase spectrophotometryrare earth elements

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岳阳县市场检验检测中心,湖南 岳阳 414100

石蜡 8-羟基喹啉 固相光度法 稀土元素

2024

山东化工
山东省化工研究院 山东省化工信息中心

山东化工

影响因子:0.249
ISSN:1008-021X
年,卷(期):2024.53(7)
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