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关于改变COD预制试剂测定煤直接液化生产污水的使用方法探究

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为降低煤直接液化生产污水COD项目检测和COD废液处理的双重高成本,同时提高试剂的利用率,针对煤制油的生产废水进行了专门实验分析探究。在预制试剂量程允许的范围内,低量程平分一支试剂,高量程连续使用同一支试剂先后分析两次。实验结果发现平分试剂,取样量减半,不影响测定结果。高量程同一水样两次测定结果虽不相同,呈递减趋势,但是减小的趋势呈一定的规律性,第二次的测定结果是第一次测定结果的90。31%~91。82%。所以,在仪器误差和方法误差允许的范围内,第二次的测定结果虽然偏小,但偏小的幅度是有据可循的。在方法、仪器以及实际生产情况允许的范围内,通过改变COD试剂的常规使用方法,可以提高COD试剂的使用率、节约购买和后期的处理成本,同时降低六价铬以及其他成分对环境的污染。
Study on the Use Method of Changing COD Prefabricated Reagent to Determine Wastewater from Coal Direct Liquefaction Production
In order to reduce the double high cost of COD project detection and COD liquid waste treatment of coal direct liquefication production wastewater,and improve the utilization rate of reagents,special experimental analysis was carried out for coal to oil production wastewater.In the range allowed by the prefabricated reagent range,the low range is divided into one reagent drug,and the high range is analyzed with the same reagent for two consecutive times.The results show that the reagent is equally divided and the sampling amount is halved,which does not affect the determination result.Although the results of two tests of the same water sample with high range are different,they show a decreasing trend,but the decreasing trend shows a certain regularity.The results of the second test are 90.31%~91.82%of the results of the first test.Therefore,within the scope of instrument error and method error,although the second measurement result is small,the amplitude of the small is evidence-based.Within the scope permitted by the method,instrument and actual production situation,by changing the conventional use method of COD reagent,the utilization rate of COD reagent can be improved,the cost of purchase and later treatment can be saved,and the environmental pollution of hexvalent chromium and other components can be reduced.

COD precast reagentmethod of useutilization ratemeasuring range

冀淑芬、左志明

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鄂尔多斯煤制油质量检验中心,内蒙古 鄂尔多斯 017200

COD预制试剂 使用方法 利用率 量程

2024

山东化工
山东省化工研究院 山东省化工信息中心

山东化工

影响因子:0.249
ISSN:1008-021X
年,卷(期):2024.53(7)
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