首页|锂电池三元正极材料生产废水回收锂的试验研究及工艺设计

锂电池三元正极材料生产废水回收锂的试验研究及工艺设计

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以锂电池三元正极材料生产废水为研究对象,通过试验,验证了碳酸钠沉淀法回收锂的工艺可行性,并得到了沉锂的最优工艺条件:反应温度为85 ℃,反应时间为70 min,碳酸钠加入量为理论的1。1倍,碳酸钠浓度为250 g/L,搅拌速度为200 r/min。经重复性试验证明,该工艺稳定可靠,单次沉锂,锂的回收率大于85%。并基于此条件,对锂电池三元正极材料生产废水回收锂的工艺进行了设计,可为锂电池三元正极材料生产废水回收锂工程应用提供指导。
Experimental Research and Process Design of Lithium Recovery from Wastewater in Production of Ternary Cathode Materials for Lithium Batteries
This study focuses on the wastewater generated during the production of ternary cathode materials for lithium batteries.Through experimental verification,the feasibility of lithium recovery using the sodium carbonate precipitation method was confirmed.The optimal process conditions for lithium precipitation were determined as follows:the reaction temperature of 85 ℃,the reaction time of 70 min,the sodium carbonate dosage at 1.1 times the theoretical amount,the sodium carbonate mass concentration of 250 g/L,and the stirring speed of 200 r/min.Repeated tests demonstrated that this process is stable and reliable with an achieved lithium recovery rate exceeding 85%.Based on these findings,a design for recovering lithium from wastewater in the production of ternary cathode materials for lithium batteries has been proposed to provide guidance for future engineering applications.

lithium settlinglithium recoveryternary cathode materialwastewaterprocess design

张永伟

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长沙矿冶研究院有限责任公司,湖南长沙 410012

沉锂 锂回收 三元正极材料 废水 工艺设计

2024

山东化工
山东省化工研究院 山东省化工信息中心

山东化工

影响因子:0.249
ISSN:1008-021X
年,卷(期):2024.53(12)
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