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白云鄂博黑云母精矿综合利用试验研究

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以白云鄂博黑云母精矿为主要原料,通过焙烧、水热浸取,富集铁、铝组分,剩余组分可作缓释肥原料.确认优化焙烧条件为:碱矿比0.8,反应温度900 ℃;最佳浸取条件为:水热温度为250℃下水浸,Fe、Al组分的浸出率分别达到98.5%和94.1%.最终通过X射线粉晶衍射、ICP-AES、扫描电子显微镜分析确认:焙烧产物的主要固相为硅酸钾镁、硅铁钠钾石以及碳酸钾;浸取产物的主要固相为氢化钠镁、金云母、羟硅钙石.
Experimental Study on Comprehensive Utilization of Bayan Obo Biotite Concentrate
With biotite concentrate produced in Bayan Obo as the main raw material,through roasting,hydrothermal leaching and enriching iron and aluminum components,the remaining components can be used as slow-release fertilizer.It is confirmed that the optimized roasting conditions are alkali ore ratio 0.8,reaction temperature 900 ℃;the best extraction condition is water thermal temperature is 250 ℃,and the leaching rate of Fe and Al components reaches 98.5%and 94.1%respectively.According to X-ray powder diffraction,ICP-AES,the main solid phase of roasting products are potassium silicate,sodium silica and potassium carbonate,and the main solid phase of extraction products is sodium magnesium hydroxide,phlogopite and hydroxysilica.

biotiteroastingextractionslow release fertiliz

董成、孙永兴、王智华、杨婷婷

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北方民族大学材料科学与工程学院,宁夏银川 750030

北方民族大学基础实验教学与实训中心,宁夏银川 750030

黑云母 焙烧 浸取 缓释肥

2024

山东化工
山东省化工研究院 山东省化工信息中心

山东化工

影响因子:0.249
ISSN:1008-021X
年,卷(期):2024.53(13)