Research on Micro Channel Synthesis Process of Methyl Ethyl Ketone Peroxide
This article studies the synthesis process of continuous production of methyl ethyl ketone peroxide,which is based on the efficient mixing characteristics of micro channel micro-scale.It utilizes the advantages of micro channel reactors such as low liquid storage,fast reaction speed,good heat transfer effect,corrosion resistance,no amplification effect in synthesis,and heat release dispersion to synthesize methyl ethyl ketone peroxide,making up for the shortcomings of intermittent reactions of methyl ethyl ketone peroxide.I have achieved continuous production of methyl ethyl ketone peroxide by optimizing residence time,molar ratio of hydrogen peroxide to butanone,reaction temperature,catalyst,etc.Solved the safety problem of heat release concentration in the intermittent reaction production of methyl ethyl ketone peroxide,achieving intrinsic safety and green production without waste water in the production of methyl ethyl ketone peroxide.There is no difference in the active oxygen content between the continuous synthesis of methyl ethyl ketone peroxide using microchannel technology and the industrial production of methyl ethyl ketone peroxide using intermittent reactions,and there is basically no difference between resin gel and curing data.
methyl ethyl ketone peroxidemicro-channel reactioncontinuous production process
万方数据
维普
