山东化工2024,Vol.53Issue(16) :165-166.

电感耦合等离子体原子发射光谱法检测钛合金中Fe、Al、V含量

Determination of Fe,Al and V in Titanium Alloy by Inductively Coupled Plasma-Atomic Emission Spectrometry

姜晨阳 刘书畅 王妙 战佳慧 鲁刚
山东化工2024,Vol.53Issue(16) :165-166.

电感耦合等离子体原子发射光谱法检测钛合金中Fe、Al、V含量

Determination of Fe,Al and V in Titanium Alloy by Inductively Coupled Plasma-Atomic Emission Spectrometry

姜晨阳 1刘书畅 1王妙 1战佳慧 1鲁刚1
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作者信息

  • 1. 威海市食品药品检验检测研究院,山东威海 264200
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摘要

建立了电感耦合等离子体原子发射光谱仪(ICP-AES)检测钛合金中铁(Fe)、铝(Al)、钒(V)含量的方法.采用氢氟酸(1+1)进行溶解.经测定,3种元素在0~60 mg/L范围内呈线性关系,相关系数为0.999,方法检出限为2~5 μg/L,相对标准偏差(RSD)为0.52%~2.51%(n=6),加标回收率为98%~101%,对标准物质进行测定,相对误差为0.5%~1.2%,结果较为满意.

Abstract

The contents of iron(Fe),aluminum(Al)and vanadium(V)in titanium alloy were determined by inductively coupled plasma-atomic emission spectrometry(ICP-AES).Dissolve the sample with(1+1)hydrofluoric acid.The mass concentration of the three elements was liner in the range of 0~60 mg/L,the correlation coefficient was 0.999,and the detection limits were 2~5μg/L,the relative standard deviations were 0.52%~2.51%(n=6),and the recoveries were 98%~101%,The relative error of the reference material was 0.5%~1.2%,and the results were satisfactory.

关键词

电感耦合等离子体原子发射光谱法/钛合金///

Key words

ICP-AES/titanium alloy/Fe/Al/V

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出版年

2024
山东化工
山东省化工研究院 山东省化工信息中心

山东化工

影响因子:0.249
ISSN:1008-021X
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